合成温度对聚苯胺性能的影响

Salma Bilal, Adil Jehan, S. Rahman, A. Shah
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引用次数: 3

摘要

研究了合成温度对掺杂十二烷基苯磺酸(PANI-DBSA)的聚苯胺收率、热稳定性、表面形貌、结晶度和电导率的影响。分别在5、10、20、25和30℃的温度下合成了聚苯胺- dbsa,并测定了产物的收率。利用热重分析(TGA)、扫描电镜(SEM)、x射线衍射(XRD)、紫外可见分光光度法(uv -可见分光光度法)和循环伏安法(CV)考察了合成聚合物的不同理化性质随合成温度的变化
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Effect of Synthesis Temperature on Properties of Polyaniline
The effect of synthesis temperature on percentage yield, thermal stability, surface morphology, crystallinity, and conductivity of polyaniline doped with dodecylbenzenesulfonic acid (PANI-DBSA) was studied. PANI-DBSA was synthesized at and the 5, 10,20, 25 and 30 0C and the percent yield of the product was determined. Furthermore, thermo gravimetric analysis (TGA), scanning electron microscopy (SEM), X-ray diffraction (XRD), UV-Visible spectrophotometry and cyclic voltammetry (CV) were utilized to inspect the variation in different physicochemical properties of the synthesized polymer with changing synthesis temperature
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