CAT on MOUSE: Control and automation of temperature for single-sided NMR instruments such as NMR-MOUSE

IF 1.9 3区 化学 Q3 CHEMISTRY, MULTIDISCIPLINARY Magnetic Resonance in Chemistry Pub Date : 2023-06-21 DOI:10.1002/mrc.5376
Sarah Mailhiot, Otto Mankinen, Jing Li, Yashu Kharbanda, Ville-Veikko Telkki, Mateusz Urbańczyk
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Abstract

Temperature-dependent experiments are a rapidly growing area of interest for low-field NMR. In this work, we present a new device for wide-range temperature control for single-sided NMR instruments. The presented device, called CAT, is simple to build, inexpensive, and easy to modify to accommodate different samples. We present the capabilities of the device using a freezing temperature study of acetic acid/water mixtures. Additionally, we present the stability of the device over long measurement times. We believe that by introducing such a device with an open-source design, we allow researchers to use it in a wide range of applications and to fully incorporate variable-temperature studies in the world of single-sided instruments.

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CAT on MOUSE:单面 NMR 仪器(如 NMR-MOUSE)的温度控制和自动化
与温度相关的实验是低场核磁共振研究中一个迅速发展的领域。在这项工作中,我们提出了一种用于单面 NMR 仪器宽范围温度控制的新装置。该装置名为 CAT,制造简单,价格低廉,易于改装以适应不同的样品。我们通过对醋酸/水混合物的冻结温度研究来介绍该装置的功能。此外,我们还介绍了该装置在长时间测量中的稳定性。我们相信,通过引入这种开源设计的设备,我们可以让研究人员在广泛的应用中使用它,并将变温研究完全融入单面仪器的世界中。
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来源期刊
CiteScore
4.70
自引率
10.00%
发文量
99
审稿时长
1 months
期刊介绍: MRC is devoted to the rapid publication of papers which are concerned with the development of magnetic resonance techniques, or in which the application of such techniques plays a pivotal part. Contributions from scientists working in all areas of NMR, ESR and NQR are invited, and papers describing applications in all branches of chemistry, structural biology and materials chemistry are published. The journal is of particular interest not only to scientists working in academic research, but also those working in commercial organisations who need to keep up-to-date with the latest practical applications of magnetic resonance techniques.
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