Novel calcium silicate based dental material with the addition of biologically active soy compound

Djordje Antonijević, K. Zelic, M. Djuric
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引用次数: 1

Abstract

Calcium silicate cements (CSC) present numerous properties that favor its use in dentistry. The purpose of this study was to investigate how the addition of soy extract affects porosity and wettability of the CSC. Soy was added to commercially available CSC named Portland cement (Italcementi, Spa Bergamo, Italy) at 10 weight % Pure Portland cement was used as a control material. Particle cement size was determined using scanning electron microscopy (TESCAN Mira3 XMU, USA Inc). Porosity of the cement was measured using micro computed tomography (μCT) (Skyscan 1172, Bruker, Belgium) at 10 μm isotropic resolution. Wettability of the cements was tested using contact angle analyzer and Endomethasone (Saint Maur, Cedex, France). Scanning electron microscopy has shown that Portland cement is composed of spherical and rods like particles ranging in size from 1 μm to 10 μm. The μCT analysis revealed that the addition of soy leads to an increased cement's porosity. Both open and closed porosity values were higher in Portland cement with soy addition than in pure Portland cement. More than 70% of pores were in the range of 20-57 μm in both investigated groups. The addition of soy resulted in lower contact angles of Endomethasone on the cement surface, suggesting that this cement formulation possesses superior wettability. It can be deduced that soy is a promising candidate for Portland cement adhesive properties improvements.
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添加生物活性大豆化合物的新型硅酸钙基牙科材料
硅酸钙胶合剂(CSC)具有许多特性,有利于其在牙科中的应用。本研究的目的是探讨大豆提取物的加入如何影响CSC的孔隙度和润湿性。大豆以10%的重量添加到商用CSC波特兰水泥(Italcementi, Spa Bergamo, Italy)中,纯波特兰水泥作为对照材料。采用扫描电子显微镜(TESCAN Mira3 XMU, USA Inc)测定水泥颗粒尺寸。采用微计算机断层扫描(μCT) (Skyscan 1172, Bruker, Belgium)在10 μm各向同性分辨率下测量水泥的孔隙度。使用接触角分析仪和endomemethasone (Saint Maur, Cedex, France)测试水泥的润湿性。扫描电镜结果表明,硅酸盐水泥由1 μm ~ 10 μm的球形和棒状颗粒组成。μCT分析结果表明,大豆的加入导致水泥孔隙度增大。掺入大豆的硅酸盐水泥的开孔率和闭孔率均高于纯硅酸盐水泥。两组孔隙在20 ~ 57 μm范围内的占比均超过70%。大豆的加入降低了内多米松在水泥表面的接触角,表明该水泥配方具有优越的润湿性。由此可以推断,大豆是改善硅酸盐水泥胶粘剂性能的有希望的候选材料。
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