Bonding performance of self-adhesive luting agents to highly translucent zirconia ceramics

Toyoaki Kobayashi, T. Takagaki, R. Takahashi, M. Ikeda, J. Tagami
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Abstract

Purpose: The purpose of this study was to evaluate the long-term durability of the bonds between self-adhesive luting agents and yttria-stabilized partially stabilized zirconia (Y-PSZ) and the effect of phosphoric acid etching as a surface pre-treatment to Y-PSZ. Materials and Methods: A total of 180 Y-PSZ disks were divided into two groups; the control group and the phosphoric acid etching group prior to the bonding with one of three self-adhesive luting agents; Panavia SA Cement Plus Automix (SAP), RelyX Unicem2 Automix (UC2), or Maxcem Elite Chroma (MXE). Bonded specimens were stored in distilled water, for 1 day, 30 days, or 150 days. After storage, the tensile bond strength was measured using a universal testing machine. The data were statistically analyzed using Welch's t -test and Welch's t -test with Bonferroni correction ( α = 0.05). Results: The tensile bond strength of each luting agent measured more than 15 MPa after 1 day of immersion in distilled water with or without phosphoric acid etching. There were no significant differences between SAP and UC2 after 30 days and 150 days ( p > 0.05) of immersion. SAP and UC2 showed significantly higher bond strength than MXE after 30 days and 150 days (p < 0.05) of immersion. There were no significant differences between with/without phosphoric acid etching in all groups ( p > 0.05). agent to Y-PSZ was material-dependent. A surface pre-treatment with phosphoric acid etching to Y-PSZ did not affect the bond strength of self-adhesive luting agent to Y-PSZ. (Asian Pac J Dent 2020; 20: 29-33. doi: 10.47416/apjod.20-0276)
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高半透明氧化锆陶瓷的自粘粘接性能研究
目的:研究自粘粘剂与钇稳定部分稳定氧化锆(Y-PSZ)之间的长期粘接性能,以及磷酸蚀刻对Y-PSZ表面预处理的影响。材料与方法:将180个Y-PSZ椎间盘分为两组;对照组和磷酸蚀刻组事先用三种自粘粘接剂中的一种粘接;Panavia SA Cement Plus Automix (SAP), RelyX Unicem2 Automix (UC2)或Maxcem Elite Chroma (MXE)。将粘接后的标本保存于蒸馏水中,分别保存1天、30天、150天。储存后,用万能试验机测定拉伸粘结强度。采用Welch’st检验和Welch’st检验并进行Bonferroni校正(α = 0.05)。结果:经磷酸蚀刻或不经磷酸蚀刻的蒸馏水浸泡1 d后,各腐蚀剂的抗拉强度均大于15 MPa。浸泡30 d和150 d后,SAP和UC2无显著差异(p < 0.05)。浸泡30 d和150 d后,SAP和UC2的结合强度显著高于MXE (p < 0.05)。各组经磷酸刻蚀组与未经磷酸刻蚀组间差异无统计学意义(p < 0.05)。对Y-PSZ的作用是物质依赖的。磷酸蚀刻Y-PSZ的表面预处理不影响自粘剂与Y-PSZ的结合强度。(亚太学报2020;20: 29-33。doi: 10.47416 / apjod.20 - 0276)
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