Investigation of firing temperature variation in ovens for ceramic-fused-to-metal dental prostheses using swept source optical coherence tomography

R. Todor, M. Negruțiu, C. Sinescu, F. Topala, A. Bradu, Virgil-Florin Duma, M. Rominu, A. Podoleanu
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Abstract

One of the most common fabrication techniques for dental ceramics is sintering, a process of heating of the ceramic to ensure densification. This occurs by viscous flow when the firing temperature is reached. Acceptable restorations require the alloy and ceramic to be chemically, thermally, mechanically, and aesthetically compatible. Thermal and mechanical compatibility include a fusing temperature of ceramic that does not cause distortion of the metal substructure. Decalibration of ovens used for firing of the ceramic layers for metal ceramic dental prostheses leads to stress and cracks in the veneering material, and ultimately to the failure of the restoration. 25 metal ceramic prostheses were made for this study. They were divided in five groups, each sintered at a different temperature: a group at the temperature prescribed by the producer, two groups at lower and two groups at higher temperatures set in the ceramic oven. An established noninvasive biomedical imaging method, swept source (SS) optical coherence tomography (OCT) was employed, in order to evaluate the modifications induced when using temperatures different from those prescribed for firing the samples. A quantitative assessment of the probes is performed by en-face OCT images, taken at constant depths inside the samples. The differences in granulation, thus in reflectivity allow for extracting rules-of-thumb to evaluate fast, by using only the prostheses currently produced the current calibration of the ceramic oven. OCT imaging can allow quick identification of the oven decalibration, to avoid producing dental prostheses with defects.
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扫描源光学相干断层扫描研究陶瓷熔接-金属牙体烤炉烧成温度变化
牙科陶瓷最常见的制造技术之一是烧结,这是一种加热陶瓷以确保致密化的过程。当达到烧成温度时,这是通过粘性流动发生的。可接受的修复要求合金和陶瓷在化学、热、机械和美学上兼容。热和机械兼容性包括不引起金属子结构变形的陶瓷熔合温度。用于烧制金属陶瓷口腔修复体陶瓷层的烤炉的校准导致贴面材料的应力和裂纹,最终导致修复失败。本研究制作了25个金属陶瓷假体。它们被分成五组,每组在不同的温度下烧结:一组在生产商规定的温度下烧结,两组在较低的温度下烧结,两组在陶瓷炉中设定的较高温度下烧结。采用一种已建立的无创生物医学成像方法,扫描源(SS)光学相干断层扫描(OCT),以评估当使用不同于规定发射样品的温度时引起的修饰。探针的定量评估是通过在样品内部恒定深度拍摄的正面OCT图像进行的。造粒的差异,从而在反射率允许提取经验法则快速评估,通过只使用目前生产的陶瓷炉当前校准的假体。OCT成像可以快速识别烤箱失标,避免生产有缺陷的义齿。
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