Extraction And Characterization Of Castor Seed Oil

A. Abitogun, O. J. Alademeyin, D. Oloye
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引用次数: 49

Abstract

The castor seeds used for this work were obtained in a market at Esa-Oke town in the western part of Osun State of Nigeria. The seeds were prepared for use by removing the endocarp, sun-drying for five days and milled to flour. A soxhlet extraction was used for the extraction of the oil and the solvent used was hexane . The oil was recovered by simple distillation. The residual oil obtained was investigated for physicochemical parameters and fatty acid composition. The result shows that : moisture content (0.300± 0.01%), specific gravity (0.948± 0.02), refractive index @30C (1.792± 0.01) ,fire point (256.000± 1.20C), flash point (225.000 ± 2.10 C), smoke point (215.000 ± 1.00 C), viscosity @ 28 C (0.425 ± 0.12), pH (5.800 ± 0.00), congealing temperature (-18.000 ± 1.50 C), turbidity (5.000 ± 1.00 C). Others were free fatty acid (7.400 ±0.07% oleic acid), acid value (14.800± 0.14 % oleic acid), saponification value (178.000± 0.42mgKOH/g oil), peroxide value (158.640 ± 2.20Meq/Kg), iodine value (58.390 ± 0.71wijs), The crude oil sample was determined according to AOAC,(1984), They are within acceptable standard. The yield of 48% makes the commercialisation of the seed in Nigeria possible and profitable. Also, the result of the analysis confirms the oil to be of good quality and can find application in food industry as food additives as well as industrial purposes.
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蓖麻籽油的提取与表征
用于这项工作的蓖麻籽是从尼日利亚奥孙州西部埃萨-奥克镇的一个市场获得的。准备使用的种子是通过去除内果皮,晒干五天,磨成面粉。采用索氏萃取法提取油,溶剂为己烷。这种油是用简单的蒸馏法回收的。对所得剩余油的理化参数和脂肪酸组成进行了研究。结果表明:水分含量(0.300±0.01%)、比重(0.948±0.02)、折射率@ 30c(1.792±0.01)、燃点(256.000±1.20C)、闪点(225.000±2.10 C)、烟点(215.000±1.00 C)、粘度@ 28 C(0.425±0.12)、pH(5.800±0.00)、凝结温度(-18.000±1.50 C)、浊度(5.000±1.00 C)、游离脂肪酸(7.400±0.07%油酸)、酸值(14.800±0.14 %油酸)、皂化值(178.000±0.42mgKOH/g油)、过氧化值(158.640±2.20Meq/Kg),碘值(58.390±0.71wijs),原油样品按AOAC(1984)测定,均在合格范围内。48%的产量使该种子在尼日利亚的商业化成为可能并有利可图。分析结果表明,该油质量优良,可作为食品添加剂和工业用途。
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