Synthesis of zinc oxide nanotiles by wet chemical route assisted by microwave heating

M. Malewicz, M. Byrczek, H. Teterycz
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引用次数: 6

Abstract

In this paper a wet chemical synthesis of zinc oxide assisted by microwave heating was investigated. Two starting solutions of ZnCl2 and NaOH were mixed under different conditions. Then obtained mixture was heated in microwave reactor. Products of reaction were investigated under scanning electron microscope. Results shown that obtained white powder is crystallized nanostructures build from nano- and microscale hexagonal tiles. This structures have hierarchical constitution, where tiles create organized systems in shape of pyramid. This highly build up active surface area can be used to enhanced sensitivity and reaction time of semiconductor gas detectors.
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微波加热辅助湿化法制备氧化锌纳米瓦
研究了微波辅助湿法化学合成氧化锌的方法。将ZnCl2和NaOH两种起始溶液在不同条件下混合。然后将得到的混合物在微波反应器中加热。在扫描电镜下对反应产物进行了研究。结果表明,所制得的白色粉末是由纳米和微尺度的六边形瓦片结晶而成的纳米结构。这种结构具有等级结构,其中瓷砖创建了金字塔形状的有组织系统。这种高度积累的活性表面积可用于提高半导体气体探测器的灵敏度和反应时间。
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