Preparation and Characterization of Gd1-xSrxAlO3 Cathode for Solid Oxide Fuel Cell

M. Rajasekhar, N. Kalaivani
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Abstract

Published by Madridge Publishers Abstract Gd1-xSrxAlO3 (0 ≤ x ≤ 0.5) cathode materials are synthesized with Gd(NO3)3, Sr(NO3)2, Al(NO3)3, and aspartic acid (fuel) by assisted combustion method with heating at 550°C for 6 hours. The surface morphology of the synthesized crystalline powder is characterized by Scanning Electron Microscopy (SEM). Thus, particle size and porosity were determined. The synthesis and crystallization are followed by thermochemical techniques (TGA/DTA) studies. The synthesized materials showed reasonable electrical conductivity. These results indicate that assisted combustion method is a promising method to prepare nanocrystalline Gd1-xSrxAlO3 for solid oxide fuel cell.
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固体氧化物燃料电池用Gd1-xSrxAlO3阴极的制备与表征
摘要以Gd(NO3)3、Sr(NO3)2、Al(NO3)3和天冬氨酸(燃料)为原料,在550℃加热6小时,采用辅助燃烧法合成了Gd1-xSrxAlO3(0≤x≤0.5)正极材料。用扫描电子显微镜(SEM)对合成结晶粉末的表面形貌进行了表征。从而确定了颗粒大小和孔隙率。合成和结晶后进行热化学技术(TGA/DTA)研究。合成的材料具有良好的导电性。这些结果表明,辅助燃烧法是一种很有前途的制备固体氧化物燃料电池用纳米晶Gd1-xSrxAlO3的方法。
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