Synthesis and characterization of ZnTe nanoparticles

Sujan Dhungana, B. R. Poudel, S. K. Gautam
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引用次数: 8

Abstract

In this work, we report the ZnTe semiconductor nanoparticles (NPs) prepared by aqueous chemical precipitation method using the tellurium precursor solution with different zinc compounds. Three batches of ZnTe NPs were synthesized to study the effect of dilution on the size and phase purity of ZnTe. The influence of source compounds and concentrations of the size and structure of NPs were studied. ZnTe NPs have great applications as field-effect transistors and photodetectors. The existing controversy regarding the crystalline structure of ZnTe NPs, whether it is cubic or hexagonal, has been resolved using X-ray Diffraction (XRD) data. The ZnTe NPs possess cubic structure, which is also confirmed by Electron Diffraction (ED) pattern. The average particle size determined from XRD data with the help of Debye-Scherrer equation is about 6 nm. The particle size can be further verified by Transmission Electron Microscopy (TEM) studies.
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纳米ZnTe的合成与表征
本文报道了以含不同锌化合物的碲前驱体溶液为原料,采用水化学沉淀法制备ZnTe半导体纳米粒子。合成了三批ZnTe NPs,研究了稀释对ZnTe粒径和相纯度的影响。研究了源化合物和浓度对NPs大小和结构的影响。ZnTe NPs在场效应晶体管和光电探测器方面有很大的应用。利用x射线衍射(XRD)数据,解决了目前关于ZnTe NPs晶体结构是立方还是六边形的争议。电子衍射(ED)图也证实了ZnTe NPs具有立方结构。借助Debye-Scherrer方程,XRD数据测定的平均粒径约为6 nm。通过透射电子显微镜(TEM)研究可以进一步验证颗粒的大小。
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