Preparation of silver nanoparticles with controlled size of particles

К. Askaruly, S. Azat, A. Kerimkulova
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Abstract

In the last decades, interest has significantly increased to to studying of nanodimensional particles, in particular, nanoparticles of various metals. In the first stage it is connected with the fact that nanoworld objects significantly differthe properties from macroobjects. Besides, there is a possibility of application of nanoparticles for receiving medical and biological medicines. In this study, we synthesized silver nanoparticles with various size and UV-VIS spectrophotometry,“Master Sizer” and “Zeta Sizer” tools characterized the nano species; we have conducted a simple and rapid one-pot synthesis method to generate nine colloids of Ag-NPs in different concentrations of TSCD and FSH. In this one-pot synthesismethod, we utilized citrate as capping groups to stabilize the NPs and FeSO4•7H2O to control the formation of shapes of NPs.
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粒径可控的纳米银的制备
近几十年来,人们对纳米粒子,特别是各种金属的纳米粒子的研究兴趣显著增加。在第一阶段,它与纳米世界对象与宏对象的属性显著不同这一事实有关。此外,纳米颗粒也有可能用于接收医学和生物药物。在本研究中,我们合成了不同尺寸的银纳米粒子,并利用紫外-可见分光光度法,“Master Sizer”和“Zeta Sizer”等工具对纳米粒子进行了表征;本研究采用一锅法,在不同浓度的TSCD和FSH下制备了9种Ag-NPs胶体。在这种一锅合成方法中,我们使用柠檬酸盐作为封盖基团来稳定NPs,并使用FeSO4•7H2O来控制NPs形状的形成。
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