Synthesis, Characterization and Applications of MoO3-Fe3O4 Nanocomposite Material

M. Navgire, Akash Nagare, G. Kale, S. Bhitre
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引用次数: 1

Abstract

In the present investigation a series of MoO3-Fe3O4 nanocomposite material such as MoO3, Fe3O4, Beta cyclodextrin (b-CD) doped MoO3-Fe3O4 and Graphite doped MoO3-Fe3O4 have been synthesized successfully by co-precipitation method. Synthesized nanomaterials were characterized in detail by XRD, FT-IR, TEM-HRTEM, UV-Vis DRS techniques. The crystalline size was in the range of 10±2 nm. The activity of the prepared material as a heterogeneous catalyst was successfully tested on the organic reaction of synthesis of substituted m-Chloro-Nitrobenzene and it was found to give excellent yield.
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MoO3-Fe3O4纳米复合材料的合成、表征及应用
本研究采用共沉淀法成功合成了MoO3-Fe3O4纳米复合材料,如MoO3、Fe3O4、β -环糊精(b-CD)掺杂MoO3-Fe3O4和石墨掺杂MoO3-Fe3O4。采用XRD、FT-IR、TEM-HRTEM、UV-Vis DRS等技术对合成的纳米材料进行了详细表征。晶体尺寸在10±2 nm范围内。在取代间氯硝基苯的有机合成反应中,成功地测试了所制备的材料作为非均相催化剂的活性,并取得了良好的产率。
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