Recycling of used alginate impression materials into final polishing powder for methacrylate denture base resins

Tomokuni Waki, Toshiko Sawada, H. Ishigami, K. Shintani, K. Okuyama, Y. Tamaki
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Abstract

Purpose: The purpose of this study was to recycling diatomite from alginate impression materials and investigate its potential as an abrading agent for denture base resins. Materials and Methods: After heating hardened alginate impression materials, a lump-like solid was powdered using a mortar and a pestle. The powder (experimental sand, ES) was characterized by X-ray diffraction (XRD). To explore the suitable ES/wax ratio, three amounts (1, 3, and 5 g, corresponding to samples ES1, ES3, ES5, respectively) were blended with 6 g of casting wax. Casting wax bars without ES were also prepared as the control. In addition, commercial diatomite (reagent-grade diatomite, RD) and a commercial final polishing product for acrylic resin (TE) were examined and compared. A disk-shaped self-curing resin (diameter: 30 mm, thickness: 3 mm) was prepared as a specimen and ground by polishing paper (#800-1,000). Surface gross measurements and surface roughness values after polishing were determined using a gross meter. These surface roughness and gloss data were statistically analyzed by one-way ANOVA and Tukey’s multiple comparison test (α = 0.05). Results: Based on the XRD results, diatomite was successfully detected in the heated alginate impression material. Sample ES3 showed good performance in experimental polishing tools, and its polishing effects were almost identical to those of RD. However, ES3 was inferior to TE in terms of surface gloss, and ES0 exhibited no polishing effect. Conclusion: Within this limited study, diatomite obtained from alginate gel was found to be effective as the final polishing material in denture base resin. (Asian Pac J Dent 2021; 21: 1-6. doi: 10.47416/apjod.21-0278)
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回收利用海藻酸盐印模材料制成甲基丙烯酸酯义齿基托树脂抛光粉
目的:本研究的目的是从海藻酸盐印模材料中回收硅藻土,并探讨其作为义齿基托树脂研磨剂的潜力。材料和方法:加热硬化的藻酸盐印模材料后,用研钵和杵研磨成块状固体。用x射线衍射(XRD)对粉末(实验砂,ES)进行了表征。为探索适宜的ES/wax比例,将样品ES1、ES3、ES5分别加入6 g铸蜡,分别为1、3、5 g。制备了不含ES的铸蜡棒作为对照。此外,对工业硅藻土(试剂级硅藻土,RD)和丙烯酸树脂(TE)的工业最终抛光产品进行了测试和比较。制备了圆盘状自固化树脂(直径:30mm,厚度:3mm)作为试样,并通过抛光纸(#800- 1000)进行研磨。表面粗测量值和抛光后的表面粗糙度值用粗计测定。表面粗糙度和光泽度数据采用单因素方差分析和Tukey多重比较检验(α = 0.05)进行统计学分析。结果:根据XRD结果,在加热后的藻酸盐印模材料中成功检测到硅藻土。ES3样品在实验抛光工具中表现出良好的性能,其抛光效果与RD几乎相同,但ES3表面光泽度不如TE, ES0没有抛光效果。结论:在这项有限的研究中,从海藻酸盐凝胶中获得的硅藻土被发现是有效的义齿基托树脂的最终抛光材料。(亚太杂志2021;21日:1 - 6。doi: 10.47416 / apjod.21 - 0278)
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