PREPARATION OF BANDING MATERIALS WITH SILVER NANOPARTICLES USING VACUUM PHYSICAL DEPOSIT METHODS

Oleksii Gornostai
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引用次数: 1

Abstract

Purpose. Adapt electron beam equipment to obtain nanosized silver structures on the surface of dressings with the ability to control the size and concentration of the resulting nanoparticles (NPs). Determine the morphology, forum, size distribution and concentration of the obtained silver nanoparticles. Methodology. Modern methods of analysis are used in the work. Electron beam evaporation method with directional vapor deposition in vacuum was used to obtain nano-particles on a flat surface. To determine the structural characteristics nanoparticles: the size of the phase formations, the morphology we were used metods: dynamic light scattering (DLS); transmission electron microscopy (TEM); the con-centration of silver in dispersed systems was determined by the method of atomic emission spectrometry with induc-tively coupled plasma (NPP ISP). Results..The results of the study demonstrate the possibility of using electron-beam deposition technology of discrete nanosized silver coatings with an average particle size of 25 nm and a dispersion of 10–120 nm on the surface of sterile gauze bandages. The established patterns of structure formation can be the basis for technically controlled synthesis of metal nanoparticles on the surface of textile materials with a given concentra-tion.Existing research and industrial and industrial electron beam equipment can be easily adapted to the production of these materials. Originality. A new technological scheme of EB-PVD with directed steam flow, the efficiency of which is ≈50%, is proposed. This scheme allows the deposition of steam from the mountain to the bottom, including on flat surfaces of banding materials. Practical value. Areas of practical application of NPs and compositions based on them can be divided into the following areas: providing or enhancing antiviral and antimicrobial properties of new or existing medical devices (bandages, masks, wipes).
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真空物理沉积法制备纳米银封带材料
目的。采用电子束设备在敷料表面获得纳米级银结构,并能够控制所得到的纳米颗粒(NPs)的大小和浓度。测定所得银纳米粒子的形貌、论坛、大小分布和浓度。方法。这项工作采用了现代分析方法。采用电子束蒸发真空定向气相沉积法在平面上制备纳米颗粒。为了确定纳米颗粒的结构特征:相形成的大小、形貌我们分别采用了动态光散射(DLS)法;透射电镜(TEM);采用电感耦合等离子体原子发射光谱法测定了分散体系中银的浓度。研究结果证明了利用电子束沉积技术在无菌纱布绷带表面制备平均粒径为25 nm、分散度为10 ~ 120 nm的离散纳米银涂层的可能性。所建立的结构形成模式可以作为在给定浓度的纺织材料表面上技术控制金属纳米颗粒合成的基础。现有的研究和工业和工业电子束设备可以很容易地适应这些材料的生产。创意。提出了一种效率约为50%的定向蒸汽流EB-PVD新工艺方案。这种方案允许蒸汽从山上沉积到底部,包括在带状材料的平面上。实用价值。NPs和基于它们的组合物的实际应用领域可分为以下领域:提供或增强新的或现有医疗器械(绷带、口罩、湿巾)的抗病毒和抗菌性能。
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