EVALUATION OF EFFECT OF POLYMERIZATION TIME ON CURING DEPTH OF VARIOUS BULK FILL COMPOSITES-AN IN VITRO STUDY

P ChandruT, Najma Azhikodan, F. Peedikayil, Soni Kottayi, N Dhanesh
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Abstract

Objectives: From the time composite has been developed, it has been subjected to various changes in composition like addition of filler and initiators to yield better result. One such modification is the new bulk fill composite. However an acceptable polymerization time to maintain adequate curing depth has to be evaluated. So the aim of this in vitro study was to evaluate the effect of polymerization time on curing depth of four bulk fill flowable composites. Methods: Total of 80 cylindrical specimens were prepared, and divided into 4 groups comprising of 20 specimens in each group. These selected groups were again subdivided into 4 groups comprising of 5 specimens in each group, based on their polymerisation time. The four specimens were Group A: SDR flow (DENTSPLY), Group B: Tetric N’ Flow (Ivoclar Vivadent), Group C: Filtek bulk fill (3M) and Group D: Venus bulk fill (Heraeus Kulzer).The aluminium mold of 4mm depth and 5mm diameter was filled with composite and top surface was irradiated using Valo LED curing light with polymerisation time of 10, 20, 40, and 60seconds on respective subgroup.The microhardness of top and bottom surfaces were performed using Vickers Hardness tester under the load of 200gram for 15seconds. The depth of cure of each specimen was determined by hardness ratio method using the formula Hardness ratio=VK of bottom surface/VK of top surface.The results were statistically analysed. Results: The study results showed that all the tested bulkfill composites can be cured to an acceptable depth. Tetric N’ Flow exhibits maximum curing depth (95.28 ±0.26) at 10sec polymerisation time. Venus bulk fill showed higher depth of cure at 20 and 40sec curing time (96.79±0.39 and 97.56±0.20). SDR flow showed adequate curing depth at 20 and 40sec curing time (92.94±0.49and 93.62±0.22 respectively). Filtek bulk fill has maximum depth of cure at 40sec curing (89.10±0.79). Conclusion: Increasing polymerisation time increases the top as well as bottom micro-hardness of all tested bulk fill composites. Tetric N’ Flow maximum curing depth at 10sec curing time. Filtek bulk fill is the material with least depth of cure.
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聚合时间对不同体积填料复合材料固化深度影响的体外研究
目的:自复合材料开发以来,为了获得更好的效果,它的组成经历了各种变化,如添加填料和引发剂。一种这样的改性是新的散装填充复合材料。然而,必须评估维持足够固化深度的可接受聚合时间。因此,本实验的目的是评价聚合时间对四种体积填充可流动复合材料固化深度的影响。方法:制备80例圆柱形标本,分为4组,每组20例。这些选择的组再次细分为4组,每组5个标本,根据其聚合时间。4个标本分别为:A组:SDR flow (DENTSPLY), B组:Tetric N ' flow (Ivoclar Vivadent), C组:Filtek bulk fill (3M), D组:Venus bulk fill (Heraeus Kulzer)。在4mm深、5mm直径的铝模中填充复合材料,用Valo LED固化光照射顶面,聚合时间分别为10、20、40和60秒。采用维氏硬度计在200g载荷下测定试样的上下表面显微硬度,持续时间为15s。每个试件的固化深度采用硬度比法确定,公式为硬度比=底面VK /顶面VK。对结果进行统计学分析。结果:试验结果表明,所测堆填体复合材料均能达到可接受的固化深度。在10秒聚合时间下,Tetric N ' Flow表现出最大的固化深度(95.28±0.26)。金星体填料在20秒和40秒的固化深度较高,分别为96.79±0.39和97.56±0.20。SDR流在20秒和40秒的固化深度为92.94±0.49和93.62±0.22。Filtek散装填料在40秒固化时的最大固化深度(89.10±0.79)。结论:随着聚合时间的延长,复合材料的顶部和底部显微硬度均有所提高。在10秒固化时间下的最大固化深度。Filtek散装填料是固化深度最小的材料。
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