Effect of additives on lubrication properties of palm oil-based trimethylolpropane ester for hydraulic fluid application

Norulaina Alias, R. Yunus, A. Idris
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引用次数: 2

Abstract

Hydraulic fluids are liquids used as the motive medium in hydraulic machinery and equipment. The current interest in protecting the environment has created a demand for vegetable-based and biodegradable hydraulic fluids. However, the lubricating properties of the vegetable-based such as poor oxidative stability and high pour point have hindered their use. In this study, Trimethylolpropane (TMP) Ester or TMPE, which is derived from palm oil-based methyl ester (POME), was used as the base fluid. The objective of this research is to study the lubrication properties of the formulated TMPE (TMPE + 1.0% of Additive A), namely the pour point (PP) test, wear and friction test and filterability test. The pour point obtained from this research was 10°C before applied to the lab-scale hydraulic test rig. This reading is much higher if compared to the commercial hydraulic fluid, which has the pour point of −30°C. Nevertheless, this result was slightly comparable to the unformulated TMPE, 12°C. The wear test shows that at 15 kg load, the WSD was 1.0 mm before application (at 0 hour), with the coefficient of friction (CoF) was 0.04 as compared to the WSD of unformulated oil, 0.46 mm and CoF of 0.04. There is no data available at 15kg load for the commercial hydraulic oil compared. Meanwhile, at 40 kg load, the WSD recorded was 3.24 mm before the application compared to commercial hydraulic oil, 0.36 mm and unformulated oil, 0.64 mm. After 800 hours application, the WSD increase sharply both for 15 kg (1049 mm) and 40 kg (3364 mm). It showed that there were particles built in the formulated oil. This is supported by the filterability study.
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添加剂对棕榈油基三甲基丙烷酯液压油润滑性能的影响
液压油是在液压机械和设备中用作动力介质的液体。当前对环境保护的兴趣产生了对植物基和可生物降解液压油的需求。然而,植物基润滑油氧化稳定性差、倾点高等特性阻碍了其应用。本研究以棕榈油基甲酯(POME)为原料,制备了三甲基丙烷(TMP)酯(TMPE)作为基液。本研究的目的是研究配制的TMPE (TMPE + 1.0%添加剂A)的润滑性能,即倾点(PP)测试、磨损摩擦测试和过滤性能测试。在应用于实验室规模的水力试验台之前,本研究获得的倾点为10°C。如果与商业液压流体相比,该读数要高得多,其倾点为- 30°C。然而,该结果与未配制的TMPE(12°C)略有相似。磨损试验表明,在15 kg载荷下,应用前(0小时)WSD为1.0 mm,摩擦系数(CoF)为0.04,而未配制油的WSD为0.46 mm, CoF为0.04。在15kg负荷下没有可用的数据与商用液压油进行比较。同时,在负载为40 kg时,应用前的WSD记录为3.24 mm,而商用液压油为0.36 mm,未配制油为0.64 mm。施用800小时后,WSD分别急剧增加15公斤(1049毫米)和40公斤(3364毫米)。结果表明,配方油中含有颗粒。过滤性研究支持了这一点。
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