DEVELOPMENT OF A MULTICOMPONENT GYPSUM CEMENT BINDER USING THE METHOD OF MATHEMATICAL PLANNING OF THE EXPERIMENT

E. Lesnichenko, N. Chernysheva, M. Drebezgova, E. V. Kovalenko, A. Bocharnikov
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Abstract

: in the article, using the method of mathematical planning of the experiment, the influence of formula and technological factors on the properties of hardened multicomponent gypsum-cement binders with a mineral additive finely ground to a specific surface of 300-700 m 2 /kg of quartz sandstone crushing screening (QSS) JSC Lebedinsky Mining and Processing Industrial Complex, Gubkin, Belgorod region, Russia was determined. It has been established that the use of finely ground QSS as part of a gypsum cement binder with a ce-ment/QSS– 1/2 ratio contributes to ensuring its operational characteristics and stability of properties during solidi-fication at the required level, contributing to a decrease in the concentration of CaO in the liquid phase of the hardening system. The optimization task was to determine the conditions for the preparation of a gypsum-cement mixture with a movement of ≤ 120 mm (according to Suttord) and the beginning of the setting time of ≥ 6 min, with the provision of the maximum compressive strength of the hardened binder. An active 3-factor experiment was planned. The fol-lowing were studied: the compressive strength of hardened gypsum-cement binder samples in 2 hours of hardening – R comp2 (Y 1 ); at 28 days of age – R comp28 (Y 2 ); as well as the mobility of the gypsum–cement mixture – P (Y 3 ) and the timing of the beginning of setting - T (Y 4 ). With the help of mathematical processing of the results of experimental studies, regression equations were obtained and with the help of nomograms constructed on the basis of mathematical expressions, the rational compositions of gypsum cement compositions were graphically and analyti-cally determined.
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采用数学规划的方法研制了一种多组分石膏水泥粘结剂
本文采用实验的数学规划方法,确定了配方和工艺因素对矿物添加剂细磨至石英砂岩破碎筛分(QSS)比表面300-700 m2 /kg的硬化多组分石膏-水泥粘结剂性能的影响。研究表明,将细磨的QSS作为石膏水泥粘结剂的一部分,以ce- cement /QSS - 1/2的比例使用,有助于确保其在固化过程中的操作特性和性能稳定性达到所需水平,有助于降低硬化体系液相中CaO的浓度。优化任务是确定石膏-水泥混合料的制备条件,其移动≤120mm(根据Suttord),开始凝结时间≥6min,并提供硬化粘结剂的最大抗压强度。计划一个主动的三因素实验。研究了硬化石膏水泥粘结剂试样在硬化2h内的抗压强度- R comp2 (Y 1);28日龄R comp28 (Y 2);以及石膏水泥混合料的流动性P (y3)和开始凝结时间T (y4)。通过对实验研究结果进行数学处理,得到回归方程,并在数学表达式的基础上构建模态图,以图形化、解析化的方式确定石膏水泥组分的合理组成。
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