Evaluations of Hot Corrosion Behavior of Al2O3 Thermal Spray Coatings with ZrO2 Reinforcements on T-91 Steel

I. Singh, K. Goyal, R. Goyal
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引用次数: 2

Abstract

Different coating with varying quantities of Al2O3 and ZrO2 were fabricated on the SA213 T-91 steel using plasma spray method to study hot corrosion resistance behavior. Experiment was conducted under the molten salt environment of 60% Na2SO4-40%V2O5 at a temperature of 900℃ inside a furnace for 50 cycles. Each cycle consisted of 1hr heating and 20 min cooling at room temperature. Results were examined using the visual inspection, weight change measurement, X-ray diffraction technique and Scanning Electron Microscopy/ Energy Dispersive X-Ray Spectroscopy (SEM/ EDS) analysis. Results showed that uncoated T-91 steel was more prone to hot corrosion as compared to coated steel specimens. It was noticed that ZrO2 reinforcements in Al2O3 coating matrix helped to enhance corrosion resistance of these coatings. The corrosion resistance increased with increase in ZrO2 content in coating matrix.
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ZrO2增强Al2O3热喷涂涂层对T-91钢热腐蚀性能的评价
采用等离子喷涂法在SA213 T-91钢表面制备了不同Al2O3和ZrO2含量的涂层,研究了其耐热腐蚀性能。实验在炉内温度为900℃,60% Na2SO4-40%V2O5的熔盐环境下进行了50次循环。每个循环由室温加热1hr和冷却20min组成。采用目视检查、重量变化测量、x射线衍射技术和扫描电镜/能量色散x射线能谱(SEM/ EDS)分析对结果进行了检验。结果表明,未涂覆的T-91钢比涂覆的T-91钢更容易发生热腐蚀。在Al2O3涂层基体中加入ZrO2增强剂有助于提高涂层的耐蚀性。随着涂层基体中ZrO2含量的增加,涂层的耐蚀性提高。
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