{"title":"Investigation of the conditions for the acquisition of triple thio-compounds from the interaction of As2S5 and CuCl2","authors":"H. Imanov","doi":"10.18411/ntvesrt-03-2022-07","DOIUrl":null,"url":null,"abstract":"In this study, the conditions for obtaining the compound Cu3(AsS4)2 from the interaction of arsenic(V) sulfide with copper(II) chloride in aqueous medium at a temperature of 323-353 K were studied. The composition of the sample was studied by X-ray phase, differential thermal, thermogravimetric and chemical analysis methods. In contrast to the results of thermogravimetric analysis of the synthesized thio-compound, based on differential thermal and X-ray analysis the obtained compound melts at a temperature of 964.3 K and corresponds to the standard intensity maxima of the Cu3AsS4 compound, respectively.","PeriodicalId":104319,"journal":{"name":"Научные тенденции в эпоху стремительного развития технологий","volume":"372 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Научные тенденции в эпоху стремительного развития технологий","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.18411/ntvesrt-03-2022-07","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
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Abstract
In this study, the conditions for obtaining the compound Cu3(AsS4)2 from the interaction of arsenic(V) sulfide with copper(II) chloride in aqueous medium at a temperature of 323-353 K were studied. The composition of the sample was studied by X-ray phase, differential thermal, thermogravimetric and chemical analysis methods. In contrast to the results of thermogravimetric analysis of the synthesized thio-compound, based on differential thermal and X-ray analysis the obtained compound melts at a temperature of 964.3 K and corresponds to the standard intensity maxima of the Cu3AsS4 compound, respectively.
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