Synthesis and microstructure of thin amorphous films of the Ag–Sn–Sb–S system

N. Melnikova, V. Kolosov, V. Y. Zarubin, A. A. Yushkov, E. S. Novoselov, V. I. Pryakhina
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Abstract

Thin homogeneous amorphous films of bulk crystalline material AgSnSbS3 were obtained by thermal evaporation in vacuum. The films demonstrate stability under irradiation by focused and scanning electron beams inside transmission electron microscope at 200 Kv. Some crystalline features appeared for the sample annealed at 390 °C are characterized.Thin homogeneous amorphous films of bulk crystalline material AgSnSbS3 were obtained by thermal evaporation in vacuum. The films demonstrate stability under irradiation by focused and scanning electron beams inside transmission electron microscope at 200 Kv. Some crystalline features appeared for the sample annealed at 390 °C are characterized.
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Ag-Sn-Sb-S体系非晶薄膜的合成与微观结构
采用真空热蒸发法制备了大块晶体材料AgSnSbS3的均匀非晶薄膜。在200 Kv的透射电子显微镜聚焦和扫描电子束照射下,薄膜表现出稳定性。在390℃退火后,样品出现了一些晶体特征。采用真空热蒸发法制备了大块晶体材料AgSnSbS3的均匀非晶薄膜。在200 Kv的透射电子显微镜聚焦和扫描电子束照射下,薄膜表现出稳定性。在390℃退火后,样品出现了一些晶体特征。
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