Microstructure and Metallurgical Properties of Aluminium 7075 – T651 Alloy / B4c 4 % Vol. Surface Composite by Friction Stir Processing

R. Ramesh, N. Murugan
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引用次数: 23

Abstract

Friction stir processing (FSP) is an emerging novel, green and energy efficient processing technique to fabricate surface composites which is based on the basic principles of friction stir welding. The distinct advantages of friction stir processing are microstructural refinement, densification, homogeneity, accurate control and variable depth of the processed zone. Metal matrix composites, particularly Aluminium based metal matrix composites, reinforced with ceramics were developed as an alternative to materials with superior strength to weight ratio and strength to cost ratio, high stiffness, and thermal stability, which effect on improving wear, creep and fatigue resistance. However, these composites also suffer from low ductility and toughness due to the incorporation of ceramic reinforcements. For many applications, a combination of high surface wear resistance and high toughness of the interior bulk material required. In those situations, it is desirable that only the surface layer of components is reinforced with ceramic particles while the bulk retains the original composition and structure with higher toughness. In this paper, the details about the fabrication of Al 7075-T651 B4C surface composite by FSP to have improved surface hardness are provided. A tool made of high carbon high chromium steel and hardened to 62 HRC, having cylindrical profile was used for FSP. By using SYSTAT software regression model has been developed for predicting microhardness of processed surface composite. The fabricated surface composites were examined using optical microscope and found defect free friction stir processed zone. It was also observed that Boron Carbide particles were uniformly distributed and well bonded with the matrix alloy fabricated at high heat input condition. It was found that the average hardness of friction stir processed surface composite was 1.5 times higher than that of the base metal aluminium 7075 – T651. The increase in hardness was attributed to fine dispersion of B4C particles and fine grain size of the aluminium matrix. Friction Stir Processing [1] is a new, solid state processing technique for microstructural modifications, which was developed based on the principle of friction-stir welding (FSW). A non-consumable rotating tool with a pin and shoulder is inserted into the material and travelled along the desired path. Because of this the frictional heat is generated and the material undergoes severe plastic deformation, resulting in significant microstructural modification in the processed zone. FSP creates a region called the Nugget or Stir zone, where the refinement of microstructure takes place producing equiaxed fine grains with high grain boundaries. Figure 1 shows the step by step procedure of Friction Stir Processing. Fig.1 Friction Stir Processing (a) Rotating tool prior to contact with the plate; (b) Tool pin contacts plate creating heat; (c) Shoulder of tool contacts plate restricting further penetration while expanding the hot zone; (d) Plate moves relative to rotating tool creating a fully re-crystallized fine grain microstructure. [1] Composites [2] represent a combination of at least two chemically distinct materials with a distinct interface separating the constituents. Their high strength to weight ratio, enhanced resistance to environmental hazards, lower density, high fatigue
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铝7075 - T651合金/ B4c 4%体积表面复合材料的组织与冶金性能
搅拌摩擦加工(FSP)是基于搅拌摩擦焊接的基本原理而发展起来的一种新型、绿色、节能的表面复合材料加工技术。摩擦搅拌加工的显著优点是组织细化、致密化、均匀化、精确控制和加工区域深度可变。陶瓷增强金属基复合材料,特别是铝基金属基复合材料,作为一种具有高强度重量比、高强度成本比、高刚度和热稳定性的替代材料而得到了发展,从而提高了材料的耐磨性、抗蠕变性和抗疲劳性。然而,由于加入了陶瓷增强剂,这些复合材料的延展性和韧性也较低。对于许多应用,需要高表面耐磨性和高韧性的内部大块材料的组合。在这些情况下,希望仅用陶瓷颗粒增强组件的表层,而整体保留具有较高韧性的原始成分和结构。本文介绍了用FSP制备Al 7075-T651 B4C表面复合材料以提高表面硬度的详细情况。采用高碳高铬钢,淬硬至62 HRC的圆柱形刀具进行FSP加工。利用SYSTAT软件建立了预测加工表面复合材料显微硬度的回归模型。利用光学显微镜对制备的表面复合材料进行了检测,发现了无缺陷的搅拌摩擦加工区。在高热输入条件下,碳化硼颗粒分布均匀,与基体合金结合良好。结果表明,搅拌摩擦处理后的表面复合材料的平均硬度是母材铝7075 - T651的1.5倍。硬度的提高是由于B4C颗粒的细分散和铝基体的细粒度所致。搅拌摩擦加工[1]是基于搅拌摩擦焊接原理发展起来的一种新型的固态加工技术。将具有销和肩的非消耗性旋转工具插入到材料中并沿着所需的路径行进。因此,产生摩擦热,材料发生严重的塑性变形,导致加工区域发生显著的显微组织改变。FSP产生了一个称为熔核或搅拌区的区域,在那里微观组织发生细化,产生具有高晶界的等轴细晶粒。图1显示了搅拌摩擦加工的分步过程。图1搅拌摩擦加工(a)与板材接触前的旋转工具;(b)工具销接触板产生热量;(c)在扩大热区的同时限制进一步渗透的工具接触板肩;(d)板相对于旋转工具移动,产生完全再结晶的细晶粒微观结构。复合材料[2]代表了至少两种化学性质不同的材料的组合,具有分离成分的不同界面。其强度重量比高,增强了对环境危害的抵抗力,密度低,抗疲劳性高
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