“Green” Suzuki-Miyaura cross-coupling: An exciting mini-project for chemistry undergraduate students

Q4 Social Sciences Educacion Quimica Pub Date : 2016-04-01 DOI:10.1016/j.eq.2015.11.006
Bruna Pereira Vargas, Clarissa Helena Rosa, Diego da Silva Rosa, Gilber Ricardo Rosa
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引用次数: 5

Abstract

A three-week mini-project is described for an experimental Physical Chemistry or Organic Chemistry course. The activities include synthesis of a biphenyl (4-methoxybiphenyl) via the Suzuki-Miyaura cross-coupling reaction using an adapted domestic microwave oven. The technical skills and concepts that are typically presented in practical chemistry courses are covered, including microwave heating, separation of mixtures, TLC techniques, melting range determination, stoichiometric calculations, and GC–MS techniques.

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“绿色”铃木-宫浦交叉耦合:化学本科生的一个令人兴奋的小项目
这是一个为期三周的小项目,描述了一个实验物理化学或有机化学课程。活动包括在改装的家用微波炉上通过Suzuki-Miyaura交叉偶联反应合成联苯(4-甲氧基联苯)。本课程涵盖了实际化学课程中常见的技术技能和概念,包括微波加热、混合物分离、TLC技术、熔化范围测定、化学计量计算和GC-MS技术。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Educacion Quimica
Educacion Quimica Social Sciences-Education
CiteScore
0.70
自引率
0.00%
发文量
78
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