Effect of annealing temperature on characteristics of ZnO/CuO nanocomposite thin films

S. S. Shariffudin, N. Ibrahim, M. Sarah, H. Hashim
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引用次数: 2

Abstract

Nanoparticles ZnO/CuO composite was successfully prepared through a simple sol-gel spin coating technique. The annealing temperature was within the range of 400°C to 600°C to study its effect to the physical, optical and electrical properties to the thin films. Their characteristics were studied by field emission scanning electron microscopy (FESEM), Atomic Force Microscopy (AFM), UV-Vis spectroscopy and 2-point probes I-V measurement. The thickness and grain size increased with the annealing temperature. The direct optical bandgap observed were between 3.06 eV to 3.2 eV, which increased with the decreased of the annealing temperature. The highest conductivity was obtained for sample annealed at 400°C with a value of 0.61614 S/cm.
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退火温度对ZnO/CuO纳米复合薄膜特性的影响
通过简单的溶胶-凝胶自旋涂层技术,成功制备了纳米ZnO/CuO复合材料。退火温度在400℃~ 600℃范围内,研究其对薄膜物理、光学和电学性能的影响。采用场发射扫描电镜(FESEM)、原子力显微镜(AFM)、紫外可见光谱(UV-Vis)和两点探针I-V测量等方法对其进行了表征。随着退火温度的升高,合金的厚度和晶粒尺寸逐渐增大。观察到的直接光学带隙在3.06 ~ 3.2 eV之间,随退火温度的降低而增大。样品在400℃退火时电导率最高,为0.61614 S/cm。
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