Nanofiberization and Characterization of Silk

K. Kondoh, Y. Morimoto, K. Ogura, Seigo Murayama, D. Terada, S. Iwatsubo
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Abstract

Silk is one of the main ingredients in cosmetics, and its function is skin moisturization and protection of both hair and skin. In this study, a silk nanofiber suspension was prepared using a wet high pressure jet mill, and its properties were evaluated. The suspension was dried and observed using field-emission scanning electron microscopy, and its specific surface area was measured using the Brunauer-Emmett-Teller ( BET ) method. For these results, it was confirmed that the silk was in the form of nanofibers. The silk nanofiber suspension was then mixed with cellulose nanofibers or a carbomer, and changes in its viscoelastic properties were measured. When only a small amount of cellulose nanofibers was added, the viscosity of the suspension increased, but no precipitation was observed. In the case of the suspension being mixed with a carbomer, a silk nanofiber gel could be easily prepared. It was found that prototype cosmetics to which silk nanofibers were added could retain skin moisture for a longer time than those without silk nanofibers.
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丝绸的纳米纤维化及其表征
丝绸是化妆品的主要成分之一,它的功能是滋润皮肤,保护头发和皮肤。本研究采用湿式高压射流磨法制备了丝纳米纤维悬浮液,并对其性能进行了评价。将悬浮液干燥后用场发射扫描电镜观察,并用BET法测定其比表面积。这些结果证实了蚕丝是以纳米纤维的形式存在的。然后将丝纳米纤维悬浮液与纤维素纳米纤维或卡波姆混合,并测量其粘弹性的变化。当只加入少量纤维素纳米纤维时,悬浮液的粘度增加,但未观察到沉淀。在悬浮液与卡波姆混合的情况下,丝纳米纤维凝胶可以很容易地制备出来。研究发现,添加纳米丝纤维的原型化妆品比不添加纳米丝纤维的原型化妆品能更长久地保持皮肤水分。
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