Investigation of static and fatigue crack growth mechanism of borated stainless steel using in situ observation method

Shota Hasunuma, K. Sugawara, T. Ogawa
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Abstract

The borated stainless steel B-SUS304P-1 is used for storage and transport metal casks in the nuclear industry. According to our previous research, the boron addition reduces the fracture toughness but has a minimal effect on the fatigue crack growth. In this study, in situ laser microscopy observation during tensile, fracture toughness and fatigue crack growth tests of B-SUS304P-1 was performed to investigate the mechanism responsible for the effects of the boron addition on static and fatigue crack growth. During the tensile test, the borides were broken, but the base material remained intact. Results obtained using the digital image correlation method revealed that the strain of boride at fracture was very low compared with the macroscopic elongation of B-SUS304P-1. For the fracture toughness test, the borides in front of the crack were broken before static crack growth. The crack propagated along a zigzag path as it grew along the broken borides. Because of this crack growth mechanism, the fracture toughness was reduced by the boron addition. In contrast, for the fatigue crack growth test, only a few broken borides were observed in front of the crack because the stress intensity factor of the fatigue test was smaller than that of the fracture toughness test. The crack thus grew linearly, and the boron addition had a minimal effect on the fatigue crack growth of the stainless steel.
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硼化不锈钢静力及疲劳裂纹扩展机制的原位观察研究
硼化不锈钢B-SUS304P-1用于核工业中储存和运输金属桶。根据我们之前的研究,硼的加入降低了断裂韧性,但对疲劳裂纹扩展的影响很小。本研究通过原位激光显微观察B-SUS304P-1的拉伸、断裂韧性和疲劳裂纹扩展试验,探讨硼添加对B-SUS304P-1静态和疲劳裂纹扩展的影响机制。在拉伸试验中,硼化物被破坏,但基材保持完整。采用数字图像相关方法得到的结果表明,与B-SUS304P-1的宏观延伸率相比,硼化物在断口处的应变非常低。断裂韧性试验中,裂纹前的硼化物在静态裂纹扩展前被破坏。裂纹沿破碎的硼化物沿之字形路径扩展。由于这种裂纹扩展机制,硼的加入降低了断裂韧性。而在疲劳裂纹扩展试验中,由于疲劳试验的应力强度因子小于断裂韧性试验的应力强度因子,在裂纹前只观察到少量的硼化物断裂。添加硼对不锈钢疲劳裂纹扩展的影响最小。
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