Fabrikasi Nanofiber PVA/Fe3O4 dengan Metode Elektrospinning

Nuril Fathurin, D. Kusumawati
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Abstract

. PVA/Fe 3 O 4 nanofibers are composite materials contain magnetic materials in nanometer-sized fibers that have biocompatible, non-toxic, and high chemical stability properties. Fe 3 O 4 will be composited with Polyvinyl Alcohol (PVA) and formed into nanofibers. The purpose of this study was to analize the effect of variations in volume % concentration of Fe 3 O 4 used on PVA/Fe 3 O 4 nanofibers. Fe 3 O 4 was dissolved in dionized water using ultrasonication. The suspension Fe 3 O 4 solution was mixed with 10% PVA solution to form PVA/Fe 3 O 4 solution with Fe 3 O 4 variations of 5%, 10%, 15%, and 20%. Electrospinning process was carried out on PVA/Fe 3 O 4 solution with a voltage of 20 kV, flow rate of 5 ml/hour, distance of jet to collector is 15 cm. The results of SEM characterization can be concluded that the one that has the best morphology in this study is PVA/Fe 3 O 4 nanofiber with a concentration of 10% because it generates uniform nanofibers with the smallest diameter at this concentration, the fibers do not attach to one other, and there are no beads.
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用电旋转方法制造PVA/Fe3O4纳米纤维
。PVA/ fe3o4纳米纤维是一种在纳米纤维中含有磁性材料的复合材料,具有生物相容性、无毒、化学稳定性高等特点。将fe3o4与聚乙烯醇(PVA)复合制成纳米纤维。本研究的目的是分析不同体积%浓度的四氧化三铁对聚乙烯醇/四氧化三铁纳米纤维的影响。采用超声法将Fe - 3o - 4溶解于离子水中。将悬浮的四氧化三铁溶液与10%的PVA溶液混合形成四氧化三铁/四氧化三铁溶液,四氧化三铁的变化幅度分别为5%、10%、15%和20%。以PVA/ fe3o4溶液为原料,在电压为20 kV、流速为5 ml/h、射流至收集器距离为15 cm的条件下进行静电纺丝工艺。SEM表征结果可以得出,本研究中形貌最好的是浓度为10%的PVA/ fe3o4纳米纤维,因为在此浓度下,PVA/ fe3o4纳米纤维生成的纳米纤维均匀,直径最小,纤维之间不相互附着,也没有珠状结构。
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