{"title":"In situ analysis utilizing electrical resistance measurements when brazing cemented carbides","authors":"W. Tillmann, N. Sievers, A. Schmidt, C. Timmer","doi":"10.3139/120.111165","DOIUrl":null,"url":null,"abstract":"Abstract Usually it is not possible to observe a high temperature brazing process such as joining cemented carbides to steel with copper as filler metal. The process takes place in a vacuum chamber at high temperatures and an analysis of the joint formed is only possible in a subsequent step. In this investigation, a novel setup has been introduced to allow for an in situ measurement of the brazing process via its electrical resistance. For this, a 4wiretechnique has been applied to the specimen to precisely measure the low resistance of the joint within a range of µΩ. By choosing two different holding times at a process temperature of 1150 °C and by analyzing the ensuing joint structures, it was possible to correlate the signal measured with the on-going diffusion and bonding process. Finally, the authors have revealed that the applied current of the measurement system had a distinct effect on the joint structure formed, which could be used additionally to improve the quality of the joint.","PeriodicalId":351153,"journal":{"name":"Materials Testing-Materials and Components Technology and Application","volume":"25 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2018-04-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Testing-Materials and Components Technology and Application","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.3139/120.111165","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Abstract Usually it is not possible to observe a high temperature brazing process such as joining cemented carbides to steel with copper as filler metal. The process takes place in a vacuum chamber at high temperatures and an analysis of the joint formed is only possible in a subsequent step. In this investigation, a novel setup has been introduced to allow for an in situ measurement of the brazing process via its electrical resistance. For this, a 4wiretechnique has been applied to the specimen to precisely measure the low resistance of the joint within a range of µΩ. By choosing two different holding times at a process temperature of 1150 °C and by analyzing the ensuing joint structures, it was possible to correlate the signal measured with the on-going diffusion and bonding process. Finally, the authors have revealed that the applied current of the measurement system had a distinct effect on the joint structure formed, which could be used additionally to improve the quality of the joint.