Synthesis and Investigation of Nickel Nanoparticles

P. Baumli, L. Somlyai-Sipos, M. Czagány, D. Janovszky
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引用次数: 1

Abstract

The melting point is one of the most important thermodynamic properties of metallic materials. The melting point, that characterizes the bulk material is independent of the size in the microscopic range but will be size-dependent in the nano-range. The reason of this phenomenon is the high surface to volume ratio, thus the atoms situated on the surface play a greater role. One of the objectives of our research was to synthetize nickel nanoparticles (Ni NPs) using aqueous medium technology. The analysis of the produced particles was performed by X-ray diffraction (XRD) and Scanning electron microscopy (SEM). Furthermore, the main objective of our work was to determine the size dependence of the melting point of the produced nickel nanoparticles by differential scanning
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纳米镍的合成与研究
熔点是金属材料最重要的热力学性质之一。表征大块材料的熔点在微观范围内与尺寸无关,但在纳米范围内则与尺寸相关。产生这种现象的原因是高的表面体积比,因此位于表面的原子起着更大的作用。我们的研究目标之一是利用水介质技术合成纳米镍。用x射线衍射(XRD)和扫描电子显微镜(SEM)对所得颗粒进行了分析。此外,我们工作的主要目的是通过差示扫描确定生产的镍纳米颗粒熔点的尺寸依赖性
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