Hydrothermal synthesis and crystal structure of catena-poly[diaqua-bis(μ₂-4-((pyridin-4-ylmethyl)amino)benzoato-κ² N:O)cobalt(II)] – 4,4′-bipyridine – water (1/2/2)

IF 0.3 4区化学 Q4 CRYSTALLOGRAPHY Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-09-07 DOI:10.1515/ncrs-2023-0148

Guang-Zhen Liu, Xin Wang

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Abstract

Abstract C 23 H 23 Co 0.5 N 4 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.6428(5) Å, b = 10.3191(5) Å, c = 11.8710(6) Å, α = 86.664 ( 4 ) ∘ $86.664{(4)}^{\circ }$ , β = 69.399 ( 5 ) ∘ $69.399{(5)}^{\circ }$ , γ = 79.429 ( 4 ) ∘ $79.429{(4)}^{\circ }$ , V = 1086.90(10) Å 3 , Z = 2, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0432, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1454, T = 293(2) K.

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水热合成链-聚[双水-双(μ - 2-4-(吡啶-4-甲基)氨基)苯甲酸-κ2 N:O)钴(II)] - 4,4′-联吡啶-水(1/2/2)的晶体结构

Abstract C 23 H 23 Co 0.5 N 4 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.6428(5) Å, b = 10.3191(5) Å, c = 11.8710(6) Å, α = 86.664 ( 4 ) ∘ $86.664{(4)}^\{circ }$ , β = 69.399 ( 5 ) ∘ $69.399{(5)}^{\circ }$ , γ = 79.429 ( 4 ) ∘ $79.429{(4)}^{\circ }$ , V = 1086.90(10) Å 3 , Z = 2, R g t ${R}_\{mathit{g}\mathit{t}}$ ( F ) = 0.0432, w R r e f $w{R}_{mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1454, T = 293(2) K.

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来源期刊

Zeitschrift Fur Kristallographie-new Crystal Structures 化学-晶体学

CiteScore

0.70

自引率

66.70%

发文量

326

审稿时长

5 months

期刊介绍： Zeitschrift für Kristallographie – New Crystal Structures was founded in 1997 as spin off of Zeitschrift für Kristallographie to meet the high demand to publish results of structure determination. All publications and their submitted CIF-data are online freely available (Open Access). Zeitschrift für Kristallographie – New Crystal Structures publishes results of determination of hitherto unknown crystal structures, and refinement of previously published crystal structures. Zeitschrift für Kristallographie – New Crystal Structures provides strict but constructive refereeing system, free access to submitted cif-files, Open Access to the PDF-files of publications, as well as data deposition at FIZ Karlsruhe and CCDC Cambridge.