Evaluation of the Microhardness of Different Types of Bulk Fill Resins

Mila O. S. Viana, Thays C. S. Lopes, Matheus A. B. S. Lopes, Lilian G. S. Pires, Marta R. O. Campos, Ayrton S. Brandim
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Abstract

The constant search for the ideal restorative material causes the new formulations to aim for an increase of 4 to 5 mm, getting an improvement of its mechanical properties, for example, the organic and inorganic matrix of other materials. With this, the objective of the present study was to evaluate the microhardness of different brands of bulk fill resin. In order to perform the research, 30 specimens were prepared, with group 1 with 10 specimens of the conventional composite resin Opallis (FGM). Group 2 with 10 specimens of Oppus Bulk Fill composite resin (FGM). And group 3 with 10 specimens of the Tetric N-Ceram Bulk fill resin (Ivoclar Vivadent), all made from a preset silicon matrix. Each group was photopolymerized on the upper surface at the time indicated by the manufacturer, stored in an oven with distilled water under 37 ° C for 24 hours. After this period, they were measured with a digital caliper and submitted to the Vickers microhardness test at 5 random points on the upper surface. The values recorded by the microdurometer were taken to the statistical analysis using ANOVA test with Tukey post-test, in which it showed a statistical difference between Bulk fill Tetric N-Ceram (Ivoclar Vivadent) and Opallis (FGM) with p value<0.001, and a statistical difference between Bulk Fill Tetric N-Ceram (Ivoclar Vivadent) and Opus Bulk Fill (FGM) with a p value of 0.001. There was no difference between Opallis and Opus Bulk fill (FGM). It was concluded that Bulk Fill Tetric N- Ceram resin (Ivoclar Vivadent) obtained a lower microhardness when compared to Opallis (FGM) and Opus Bulk Fill (FGM) resins.
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不同类型填充树脂显微硬度的评价
对理想修复材料的不断探索使新配方的目标是增加4到5毫米,从而改善其机械性能,例如其他材料的有机和无机基体。因此,本研究的目的是评估不同品牌的散装填充树脂的显微硬度。为了进行研究,制备了30个样品,第一组10个样品为常规复合树脂蛋白石(FGM)。第二组为Oppus散装填充复合树脂(FGM)试件10个。第三组为10个n -陶瓷体积填充树脂(Ivoclar Vivadent)样品,均由预先设置的硅基体制成。每组在制造商指定的时间在上表面进行光聚合,用蒸馏水在37°C下的烤箱中保存24小时。这段时间后,用数字卡尺测量,并在上表面随机选取5个点进行维氏显微硬度测试。微硬度计记录的数值采用Tukey后验的ANOVA检验进行统计分析,其中Bulk fill tric N-Ceram (Ivoclar Vivadent)与Opallis (FGM)之间的p值为0.001,具有统计学差异;Bulk fill tric N-Ceram (Ivoclar Vivadent)与Opus Bulk fill (FGM)之间的p值为0.001。Opallis和Opus Bulk fill (FGM)之间没有差异。结果表明,与Opallis (FGM)和Opus Bulk Fill (FGM)树脂相比,Ivoclar Vivadent N- Ceram树脂具有较低的显微硬度。
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