Green synthesis of recyclable reduced graphene oxide-gold nanocatalyst using Alstonia scholaris: Applications in waste water purification and microbial field

Piu Das, Bapan Bairy, Sanjukta Ghosh, Raktim Ghosh, Somasri Dam, Avijit Ghorai, Moni Baskey Sen
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引用次数: 1

Abstract

Abstract The green synthetic approaches are the alternative methods for the preparation of various types of nanoparticles to keep sustainable evolution. A novel green synthesis of gold- reduced graphene oxide nanocomposites was conducted through simple heating method using Alstonia scholaris (A. scholaris) bark extract. There are several techniques that confirm the formation of the nanocomposites for synthesis of gold nanoparticles on reduced graphene oxide (RGO), such as X-ray diffraction (XRD), UV–visible spectroscopy (UV–vis) and Fourier transformed infrared spectroscopy (FT-IR). The size distributions of the gold nanoparticles (Au NPs) grown on RGO surface was measured using two different methods: particle distribution study and transmission electron microscopy (TEM) image. These two methods provided similar size distribution which is around 5–8 nm. Subsequently, the catalytic performance was evaluated by 4-nitro aniline (4-NA). The photocatalytic activities were investigated using different organic hazardous dyes, such as methylene blue (MB), methyl orange (MO) and the change of photocatalytic behaviour was shown by varying the catalyst amount and pH. The chemical oxygen demand (COD) analyses for complete removal of organic dye were carried out using the two nanocomposite samples. To perceive the effect on different bacterial strains, antibacterial and antiprotozoal studies have been carried out with this nanocomposite.
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绿色合成可回收还原型氧化石墨烯-金纳米催化剂:在废水净化和微生物领域的应用
绿色合成途径是制备各种类型纳米粒子以保持可持续进化的替代方法。以金楸树皮提取物为原料,通过简单的加热法制备了一种新型的金还原性氧化石墨烯纳米复合材料。有几种技术可以证实在还原氧化石墨烯(RGO)上合成金纳米颗粒的纳米复合材料的形成,如x射线衍射(XRD),紫外可见光谱(UV-vis)和傅里叶变换红外光谱(FT-IR)。采用颗粒分布研究和透射电子显微镜(TEM)成像两种不同的方法测量了生长在还原氧化石墨烯表面的金纳米颗粒(Au NPs)的尺寸分布。两种方法的尺寸分布相似,均在5 ~ 8 nm左右。随后,用4-硝基苯胺(4-NA)评价了催化性能。考察了亚甲基蓝(MB)、甲基橙(MO)等不同有机有害染料对纳米复合材料光催化活性的影响,并通过催化剂用量和ph的变化考察了纳米复合材料光催化性能的变化。为了了解这种纳米复合材料对不同细菌菌株的影响,研究人员利用这种纳米复合材料进行了抗菌和抗原虫研究。
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来源期刊
Advances in Natural Sciences: Nanoscience and Nanotechnology
Advances in Natural Sciences: Nanoscience and Nanotechnology Engineering-Industrial and Manufacturing Engineering
CiteScore
3.80
自引率
0.00%
发文量
60
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