Synthesis of ferromagnetic material nano powder and study of its effect on antibacterial activity

IF 1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Digest Journal of Nanomaterials and Biostructures Pub Date : 2023-10-30 DOI:10.15251/djnb.2023.184.1203
Z. M. A. Abbas, W. A. Shatti, D. S. Kalaf
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Abstract

This work is to synthesize the cobalt ferrites nano powder of with the stoichiometric formula CoxFe2O4 (x= 0.8 and 1.4) by using sol-gel auto combustion method , and study structural and magnetic properties, the ferrite powders were calcined at 500, 600, and 700 °C for 3 hrs to remove organic waste and increase homogeneity and, The XRD diffraction analysis for CoxFe2O4 nanoferrites with single spinel structure. The crystal size of the formed crystallite of ferrite specimens increases with increasing temperature calcination and cobalt content , (FE-SEM) shows agglomerated with homogenous spherical and polyhedral particles. proportion of each of Fe ,Co, and O in all specimens is confirmed using the Energy Dispersive Spectrum (EDS),the magnetic characteristics are measured with a VSM. The remanence magnetization (Mr) saturation magnetization(Ms), and magnetic moment (nB) of CoxFe2O4 nanoferrites are found to go up with increasing calcination temperature, and E-coli bacteria were used to examine the inhibition of each ferrite using the diffusion-drilling agar method, as it is known that these nano powder possess therapeutic efficacy for numerous diseases.
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铁磁材料纳米粉体的合成及其抑菌效果研究
本文采用溶胶-凝胶自燃烧法合成了化学量计公式为CoxFe2O4 (x= 0.8和1.4)的钴铁氧体纳米粉末,并对其结构和磁性能进行了研究,分别在500、600和700℃下煅烧3小时,去除有机废物,提高均匀性,对具有单尖晶石结构的CoxFe2O4纳米铁氧体进行了XRD衍射分析。铁素体试样的晶粒尺寸随着煅烧温度和钴含量的升高而增大,FE-SEM表现为球状和多面体颗粒的团聚。利用能量色散谱(EDS)确定了各试样中Fe、Co和O的比例,并用VSM测量了磁性特征。发现CoxFe2O4纳米铁氧体的剩余磁化强度(Mr)、饱和磁化强度(Ms)和磁矩(nB)随煅烧温度的升高而升高,并利用扩散钻琼脂法用大肠杆菌检测了每种铁氧体的抑制作用,因为已知这些纳米粉末对许多疾病都有治疗作用。
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来源期刊
Digest Journal of Nanomaterials and Biostructures
Digest Journal of Nanomaterials and Biostructures 工程技术-材料科学:综合
CiteScore
1.50
自引率
22.20%
发文量
116
审稿时长
4.3 months
期刊介绍: Under the aegis of the Academy of Romanian Scientists Edited by: -Virtual Institute of Physics operated by Virtual Company of Physics.
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