[Study on the physico-chemical properties of fluoride gel in application of freeze-drying gelatin gel method (tray method)].

T Endo, K Oka, H Murakami, M Yoshida, N Kosuge, A Kameda
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Abstract

As a means of studies of securing freeze-drying method by application of tray for prevention of white spots, decalcification and secondary caries of enamel, which may develop during and after orthodontic treatment, comparison and review were made on physico-chemical properties of fluoride gel to be used for gelatin gel method and freeze-drying gelatin gel method (control group gel and experimental group gel), and the following results were obtained: 1. Physical properties As the results of naked-eye observations, morphological observations through scanning electron microscope and measurements of gelly strength and viscosity, no distinct difference between control and experimental group gel was noted. 2. Chemical properties The qualitative analyses of fluoride ion with ion chromatogram and pH measurement were carried out, and consequently experimental group gel indicated similar values to control group gel. From the foregoing results, it was learned that no significant difference in their physico-chemical properties was clearly confirmed between control and experimental group gel, and it was suggested that similarly to control group gel, experimental group gel would be an effective gel substance as gel media for the formation process of fluorapatite or the reinforcement method of tooth enamel.

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[冻干明胶凝胶法(托盘法)应用氟化物凝胶的理化性质研究]。
为了预防正畸治疗中及治疗后牙釉质出现白斑、脱钙和继发性龋病,研究了托盘固定冷冻干燥法,对明胶凝胶法和冷冻干燥明胶凝胶法(对照组凝胶和实验组凝胶)使用的氟化物凝胶的理化性质进行了比较和回顾,得到以下结果:裸眼观察、扫描电镜形态学观察以及凝胶强度和粘度测量结果显示,对照组凝胶与实验组凝胶无明显差异。2. 化学性质用离子色谱法和pH测定法对氟离子进行定性分析,结果表明实验组凝胶与对照组凝胶具有相近的化学性质。从上述结果可知,实验组凝胶与对照组凝胶在理化性质上并无明显差异,提示实验组凝胶与对照组凝胶类似,将成为氟磷灰石形成过程或牙釉质加固方法的有效凝胶介质。
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