Phase transformation and deformation behavior under isothermal compression in β-quenched metastable Ti-10V-2Fe-3Al alloy

IF 4.5 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Materials Today Communications Pub Date : 2023-11-30 DOI:10.1016/j.mtcomm.2023.107727
E Zhu, Fuguo Li, Qian Zhao, Xuehan An, Siddique Farah, Kenan Yao
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Abstract

Comprehensive knowledge on the hot deformation behavior and microstructure evolution of metastable titanium alloys is critical for process optimization and microstructure regulation. The isothermal compression of β-quenched metastable titanium alloys (Ti-10V-2Fe-3Al) was experimented at different temperatures (600 ℃-800 ℃) with the strain rate of 10-3s-1 in present work. The stress-strain curves show that the flow stress reduces with increasing temperature, and the characteristics of the stress-strain curve at low temperature (600 ℃) are clearly distinct from those at other high temperatures. During the isothermal compression process at 600 °C, the deformation went through four stages: initial linear hardening (stage Ⅰ), Discontinuous yielding phenomenon (DYP, stage Ⅱ) followed by work hardening (stage Ⅲ) and final flow softening (stage Ⅳ). Further observations of the microstructure throughout each deformation stage revealed that the precipitation of αGB and the proliferation of dislocation lead to initial linear hardening behavior. The softening of deformation behavior during the discontinuous yield stage is originated from the fragmentation of αGB and the generation of a large amount of moving dislocations. Almost all β phase transformed into lamellar α phase as the deformation degree increased, which is the main cause of work hardening after discontinuous yield. The major causes of final flow softening are the formation of deformation bands and spheroidization of α phase. The present work analyses the correlation between the deformation behavior and microstructure features on the deformation mechanisms of metastable β titanium alloys and reveals the potential mechanism of metastable β alloy under thermal deformation and provides more comprehensive information for the optimization of the process parameters of hot deformation.

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β淬火亚稳Ti-10V-2Fe-3Al合金的相变及等温压缩变形行为
全面了解亚稳钛合金的热变形行为和微观组织演变对工艺优化和微观组织调控至关重要。本文对β淬火亚稳钛合金(Ti-10V-2Fe-3Al)在不同温度(600℃~ 800℃)下,应变速率为10-3s-1的等温压缩进行了实验。应力-应变曲线表明,流变应力随温度升高而减小,且低温(600℃)下的应力-应变曲线特征与其他高温下明显不同。在600℃等温压缩过程中,变形经历了4个阶段:初始线性硬化(Ⅰ阶段)、不连续屈服现象(Ⅱ阶段)、加工硬化(Ⅲ阶段)和最终流动软化(Ⅳ阶段)。进一步观察各个变形阶段的显微组织发现,αGB的析出和位错的扩散导致了初始线性硬化行为。断续屈服阶段变形行为的软化源于αGB的破碎和大量移动位错的产生。随着变形程度的增加,几乎所有的β相转变为片层α相,这是断续屈服后加工硬化的主要原因。变形带的形成和α相的球化是导致最终流动软化的主要原因。本文分析了亚稳β钛合金变形机理中变形行为与微观结构特征之间的关系,揭示了亚稳β合金在热变形作用下的潜在机理,为热变形工艺参数的优化提供了更全面的信息。
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来源期刊
Materials Today Communications
Materials Today Communications Materials Science-General Materials Science
CiteScore
5.20
自引率
5.30%
发文量
1783
审稿时长
51 days
期刊介绍: Materials Today Communications is a primary research journal covering all areas of materials science. The journal offers the materials community an innovative, efficient and flexible route for the publication of original research which has not found the right home on first submission.
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