Preparation and properties of PTFE@TiO2/epoxy superhydrophobic coating

IF 1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Digest Journal of Nanomaterials and Biostructures Pub Date : 2023-12-04 DOI:10.15251/djnb.2023.184.1433
G. Q. Xu, C. Q. Li, F. J. Wang, J. F. Ou, Z. Y. Xue, A. Amirfazli
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Abstract

The problem of bacterial adhesion has been a challenge in everyday life and industry for decades. In this paper, polytetrafluoroethylene(PTFE) micropowder, titanium dioxide(TiO2) nanopowder, ethyl acetate and epoxy resin were sequentially added to a beaker and stirred well, then the nanoparticles were modified using perfluorooctyltriethoxysilane (POTS), and finally superhydrophobic coatings were fabricated on the surface of an aluminium sheet by spraying process. Characterisation was carried out using scanning electron microscopy and contact angle measurement, and the coating wettability, chemical stability and mechanical stability properties were investigated, and finally the coating was tested for antimicrobial properties. The study suggests that the hydrophobicity of the sample was optimal at a contact angle of 163.3° and a rolling angle of 3.2° when the ratio of PTFE micropowder to nano-TiO2 by mass was 1:4 and the ration between POTS and nanoparticles by mass was 12%. The contact angles were 137.8° and 143.6° after 25 and 32 hours of soaked in an anhydrous solution with a pH of 14 and 1, respectively. Most importantly, it exhibits good antimicrobial properties.
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PTFE@TiO2/epoxy 超疏水涂层的制备与性能
几十年来,细菌粘附问题一直是日常生活和工业中的一个挑战。本文将聚四氟乙烯(PTFE)微粉、二氧化钛(TiO2)纳米粉、乙酸乙酯和环氧树脂依次加入烧杯中搅拌均匀,然后用全氟辛基三乙基氧基硅烷(POTS)对纳米颗粒进行改性,最后通过喷涂工艺在铝板表面制备超疏水涂层。通过扫描电镜和接触角测试对涂层进行了表征,考察了涂层的润湿性、化学稳定性和机械稳定性,最后对涂层进行了抗菌性能测试。研究表明,当PTFE微粉与纳米tio2的质量比为1:4,锅与纳米tio2的质量比为12%时,接触角为163.3°,滚动角为3.2°时,样品的疏水性最佳。在pH为14和1的无水溶液中浸泡25和32 h后,接触角分别为137.8°和143.6°。最重要的是,它具有良好的抗菌性能。
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来源期刊
Digest Journal of Nanomaterials and Biostructures
Digest Journal of Nanomaterials and Biostructures 工程技术-材料科学:综合
CiteScore
1.50
自引率
22.20%
发文量
116
审稿时长
4.3 months
期刊介绍: Under the aegis of the Academy of Romanian Scientists Edited by: -Virtual Institute of Physics operated by Virtual Company of Physics.
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