Ceramic-Forming Organosilicon Polymer as a Modifier of Heat-Insulating Syntactic Material

IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, CERAMICS Glass and Ceramics Pub Date : 2023-12-22 DOI:10.1007/s10717-023-00618-1
V. Yu. Chukhlanov, N. N. Smirnova, I. A. Krasilnikova, N. V. Chukhlanova
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Abstract

The results of the preparation of strengthened syntactic carbon materials that can be used for industrial-grade heat insulation in conditions of heightened pressures and temperatures are presented. Strengthened syntactic carbon material is obtained by mixing hollow carbon microspheres, pre-treated with vanadium (III) chloride catalyst, with a phenol-formaldehyde binder with the addition of fine polydimethylsilane, molding the composition at low pressure, soaking the mold at 150°C for 2 h, followed by heat treatment in an inert environment at 375°C and final carbonization in combination with carbidization when the temperature rises at a rate of 100 K/h to 900°C. The physicomechanical and thermophysical characteristics were studied. Syntactic material can be used for the manufacture of heat-insulation products operating at high temperatures.

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作为隔热合成材料改性剂的陶瓷成型有机硅聚合物
本文介绍了可在高压和高温条件下用于工业级隔热的强化合成碳材料的制备结果。强化合成碳材料的制备方法是:将用氯化钒(III)催化剂预处理过的空心碳微球与添加了精细聚二甲基硅烷的苯酚-甲醛粘合剂混合,在低压下成型,在 150°C 下浸泡 2 小时,然后在 375°C 的惰性环境中进行热处理,最后在温度以 100 K/h 的速度升至 900°C 时结合碳化进行碳化。对其物理机械特性和热物理特性进行了研究。合成材料可用于制造在高温下工作的隔热产品。
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来源期刊
Glass and Ceramics
Glass and Ceramics 工程技术-材料科学:硅酸盐
CiteScore
1.00
自引率
16.70%
发文量
85
审稿时长
6-12 weeks
期刊介绍: Glass and Ceramics reports on advances in basic and applied research and plant production techniques in glass and ceramics. The journal''s broad coverage includes developments in the areas of silicate chemistry, mineralogy and metallurgy, crystal chemistry, solid state reactions, raw materials, phase equilibria, reaction kinetics, physicochemical analysis, physics of dielectrics, and refractories, among others.
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