Effects of Annealing Soaking Time on Carbide Precipitates and Mechanical Properties of As-Cast Thin Wall Ductile Iron

E. F. Ochulor, S. Adeosun, Ademola Joseph Kareem, Ajibola Ikeoluwa Ashade
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Abstract

Thin Wall Ductile Irons (TWDI) are viable material option in the automotive industry due of their good castability, adequate mechanical properties, wear resistance, good machinability and fatigue properties. However due to size reduction and increased cooling rate, carbide precipitates occur in the as-cast microstructure of TWDIs, impacting negatively on mechanical properties, nodularity and nodule count. Heat treatment processes that reduce or eliminate these carbide phases can be adopted to remedy such defects. In this study, 4 mm TWDI samples cast in green sand moulds, showing carbide precipitation in microstructure were subjected to an Annealing heat treatment by austenizing to 920oC and varying soaking times of 5, 10, 15, 20, 25 and 30 minutes, afterwards they were cooled in the furnace to room temperature. Microstructural analysis and mechanical property tests were carried out in all the samples via Optical microscopy (OM) and Scanning electron microscopy (SEM), hardness and tensile tests. Microstructure of heat-treated samples showed significant reduction of carbide precipitates in comparison with their as cast counterpart. It was observed that the soaking time impacted on carbide precipitation reduction. Hardness values reduced from 291.6 Hv in the as cast sample to 247.8 Hv and 243.5 Hv for samples soaked for 25 and 30 minutes respectively, whereas tensile strength reduced progressively from 596 MPa to 544 MPa for as cast to 30 minutes soaking time respectively. Percent elongation increased from 4.3 % elongation for the as cast sample to 8.7 % elongation in the sample with soaking time of 30 minutes at 920 oC. This study has shown that carbide precipitation can be significantly reduced by adopting the annealing treatment parameters outlined above.
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退火浸泡时间对铸造薄壁球墨铸铁碳化物析出物和机械性能的影响
薄壁球墨铸铁(TWDI)具有良好的可铸性、足够的机械性能、耐磨性、良好的机加工性能和疲劳性能,因此是汽车工业中可行的材料选择。然而,由于尺寸减小和冷却速度增加,TWDI 的铸造微观结构中会出现碳化物析出物,从而对机械性能、结核性和结核数量产生负面影响。可采用减少或消除这些碳化物相的热处理工艺来弥补这些缺陷。在这项研究中,对在绿砂模具中铸造的 4 毫米 TWDI 样品进行了退火热处理,奥氏体化温度为 920 摄氏度,浸泡时间分别为 5、10、15、20、25 和 30 分钟,然后在炉中冷却至室温。通过光学显微镜(OM)和扫描电子显微镜(SEM)、硬度和拉伸试验对所有样品进行了微观结构分析和机械性能测试。与铸造样品相比,热处理样品的微观结构显示碳化物析出物明显减少。据观察,浸泡时间对碳化物析出的减少有影响。硬度值从铸造样品的 291.6 Hv 分别降至浸泡 25 分钟和 30 分钟样品的 247.8 Hv 和 243.5 Hv,而抗拉强度则从铸造样品的 596 兆帕逐渐降至浸泡 30 分钟样品的 544 兆帕。在 920 oC 下浸泡 30 分钟的试样中,百分比伸长率从原样的 4.3% 增加到 8.7%。这项研究表明,采用上述退火处理参数可显著减少碳化物析出。
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