Comparison of Shear Bond Strength in Novel Calcium Silicate-Based Materials to Composite Resin

Wonkyu Shin, Hyuntae Kim, Ji-Soo Song, T. Shin, Young-Jae Kim, Jung‐Wook Kim, Ki-Taeg Jang, H. Hyun
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Abstract

The purpose of this study was to evaluate whether the newly introduced calcium silicate-based materials with fast-setting properties could be appropriately used as basement materials in indirect pulp treatment (IPT). This was performed by quantifying the durability of adhesion between the material and composite resin, measured by the shear bond strength (SBS). Five calcium silicate-based materials, TheraCal LC® (TLC), TheraCal PT® (TPT), TheraBase® (TB), Well-Root™ PT (WPT), and Endocem® MTA (EMTA), as well as two glass ionomer-based materials, Fuji II and Fuji II LC, were included. Specimens containing these materials were manufactured and bonded to composite resin with a universal adhesive applied in self-etch mode. The SBS values and failure modes were recorded, and the mean SBSs of the materials were compared. Both TPT and TB exhibited SBS values that were similar to TLC, while both WPT and EMTA appeared to have statistically lower SBS values. Mixed failure was commonly observed in TLC and TPT, while all WPT and EMTA samples showed cohesive failure. In comparison with TLC and TPT, more samples with cohesive failure were observed in TB, implying that this material forms a stronger bond with composite resin. Together with the ability of TB to chemically bind to dentin due to its 10-methacryloyloxydecyl dihydrogen phosphate component, TB seems to be a promising material for IPT within the limitations of this in vitro study.
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新型硅酸钙基材料与复合树脂的剪切粘接强度比较
本研究的目的是评估新推出的具有快速固化特性的硅酸钙基材料是否可以适当地用作间接牙髓治疗(IPT)的基底材料。具体方法是通过剪切粘接强度(SBS)来量化材料与复合树脂之间粘接的耐久性。研究对象包括五种硅酸钙基底材料:TheraCal LC® (TLC)、TheraCal PT® (TPT)、TheraBase® (TB)、Well-Root™ PT (WPT) 和 Endocem® MTA (EMTA),以及两种玻璃离聚物基底材料:Fuji II 和 Fuji II LC。制作了含有这些材料的试样,并用通用粘合剂以自酸蚀模式粘合到复合树脂上。记录了 SBS 值和失效模式,并比较了材料的平均 SBS 值。TPT 和 TB 的 SBS 值与 TLC 相似,而 WPT 和 EMTA 的 SBS 值在统计上似乎较低。TLC 和 TPT 通常会出现混合破坏,而所有 WPT 和 EMTA 样品都会出现内聚破坏。与 TLC 和 TPT 相比,TB 中出现内聚失效的样品更多,这意味着这种材料与复合树脂形成的粘合力更强。再加上 TB 的 10-甲基丙烯酰氧癸基磷酸二氢酯成分能够与牙本质发生化学结合,因此在这项体外研究的局限性范围内,TB 似乎是一种很有前途的 IPT 材料。
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