RESEARCH OF INJECTION METHODS FOR Y2O3 NANOPARTICLES INTO NICKEL- FREE STAINLESS STEEL DURING INDUCTION VACUUM REMELTING

Alexandr Panichkin, F.E. Popov, N. Lutchenko, Askhat Beldeubayev, Ivan Samokhvalov, Alexandr Arbuz
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Abstract

Investigation of the possibility of obtaining an oxide-dispersed strengthening steel alloy based on 5 different ways of fine-dispersed strengthening particles Y2O3 injection into the liquid phase of steel Fe-13Cr (wt. %) in a vacuum. For this purpose, were conducted 5 series of experiments with different conditions and regimes. 2 series of 5 melts were carried out to evaluate the possibility of mechanical injection of yttrium oxide in the melt with different entry conditions. 3 series of 5 melts were conducted to evaluate the possibility of oxidation of metallic yttrium in the melt with the formation of yttrium oxide particles. Either melt residence or residual pressure in the furnace chamber was varied in different series. The results of ingot analysis on XRF, ICP-AES, and EDS showed that significant amounts of yttrium oxide were not injected. The method with oxidation of metallic yttrium in the melt from the reduction ofspecially added iron oxide with a concentration of 0.0552 ppm showed the best result.
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感应真空重熔过程中向无镍不锈钢中注入 y2o3 纳米粒子的方法研究
基于 5 种不同的细分散强化粒子 Y2O3 在真空中注入钢 Fe-13Cr(重量百分比)液相的方法,研究获得氧化物分散强化钢合金的可能性。为此,进行了 5 次不同条件和制度的系列实验。2 个系列共 5 次熔炼,以评估在不同进入条件下在熔体中机械注入氧化钇的可能性。进行了 3 个系列 5 次熔化实验,以评估金属钇在熔体中氧化并形成氧化钇颗粒的可能性。在不同的系列中,熔体停留时间或炉腔中的残余压力均有所不同。钢锭的 XRF、ICP-AES 和 EDS 分析结果表明,没有注入大量的氧化钇。熔液中金属钇被氧化的方法是通过还原特别添加的氧化铁(浓度为 0.0552 ppm)来实现的,结果最好。
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Journal of Chemical Technology and Metallurgy
Journal of Chemical Technology and Metallurgy Engineering-Industrial and Manufacturing Engineering
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