Evaluation the Effect of Heat Treatment on Corrosion Resistance of Cobalt Chromium Alloys

Evan H. Alwan, Sabiha M. Kanaan
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Abstract

The purpose of present study is to evaluate and comparison the effect of different milling technique surface of CAD/CAM for milled Co-Cr alloy specimens.Material and Methods: The diagnostic divides 20 disc-shaped specimens into 2 main groups, each consisting of 10 specimens for Co/Cr alloys according to their construction, the material used in hard milling and soft milling. All samples for further examination were prepared as drilled discs (diameter 15 mm, height 3 mm) whose surfaces were then finished and polishing with a diamond polisher. Scanning electron microscopy (SEM) images with energy-dispersive beam spectroscopy (EDS) were acquired for one sample in each set to assess the surface topography of the metal framework. All samples were degreased, and steam cleaned samples and heat treated in accordance with the complete firing procedure. Then scanning electron microscopy (SEM) after heating. Samples prepared in the lab for electrochemical corrosion testing were polarized and corroded in accordance with their electrical potential. Results were recorded using Levenes test and anova, with appropriate data analyzed for differences between groups. Results: The results of this study presented that the Descriptive statistics for corrosion test (mmpy) for all experimental groups revealed that the hard milling group mean was the lowest among all groups of the study is recorded (0005), followed, Group soft milling (.0071). The data were statistically analyzed using Welch’s ANOVA and Levene’s test which revealed highly significant differences (p<0.01) among groups. Conclusion: Corrosion resistance decreases in the following order: soft metal milling > hard metal milling, according to the obtained corrosion parameter values.
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评估热处理对钴铬合金耐腐蚀性的影响
本研究的目的是评估和比较 CAD/CAM 不同铣削技术表面对铣削 Co-Cr 合金试样的影响:根据钴/铬合金的结构、硬铣和软铣所使用的材料,诊断将 20 个圆盘状试样分为 2 大组,每组 10 个试样。所有用于进一步检查的试样都是钻孔圆盘(直径 15 毫米,高 3 毫米),然后用金刚石抛光机对其表面进行抛光。对每组样品中的一个样品采集了扫描电子显微镜(SEM)图像和能量色散光束光谱(EDS),以评估金属框架的表面形貌。所有样品都经过脱脂和蒸汽清洗,并按照完整的烧制程序进行热处理。然后在加热后进行扫描电子显微镜(SEM)观察。在实验室制备的用于电化学腐蚀测试的样品根据其电势进行极化和腐蚀。使用 Levenes 检验和 anova 记录结果,并对组间差异进行适当的数据分析。结果研究结果表明,所有实验组腐蚀试验(mmpy)的描述性统计显示,硬磨组的平均值在所有研究组中最低,为(0005),其次是软磨组(.0071)。使用 Welch 方差分析和 Levene 检验对数据进行了统计分析,结果表明,根据所获得的腐蚀参数值,硬金属铣削组与软金属铣削组之间存在非常显著的差异(p)。
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