Evaluation of Surface Hardness of Heat Cure Acrylic Resin Reinforce by Nano Al2O3 After Polishing with Different Materials

Nihad Hassan M, Wafaa A.Jassem
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Abstract

The goal of this research was to determine the surface hardness of heat cure acrylic resin reinforced with Nano Al2O3 after polishing with various materials. Materials and methods: - The 70 rectangular samples were made of a pink impact resistant thermoset acrylic (Vertex, Implacryl, The Netherlands) (65mm long x 10mm diameter x 3mm thick). Following polishing with each material (pumice stone, diamond suspension, colloidal silica), the surface roughness of each sample was determined using the Profilometer surface roughness instrument. The sample surface was glued to the profiler's horizontal base in a very flat position, and the stylus (the profiler's needle) was moved across each sample surface three times in three different directions over a distance of 1.7 mm. were separated into (7) groups were determined by the concentration of Nano powder, Group (A) Control without adding Nano filler of (Al2O3) (10) specimens, Group (B) Polishing with pumice Al2O3 (1%) (10) specimens, Group (C) Polishing with pumice Al2O3 (1.5 %) (10) specimens, Group (D) Polishing with Colloidal Al2O3 (1%) (10) specimens, Group (E) Polishing with Colloidal Al2O3 (1.5%) (10) specimens, Group (F) Polishing with Diamond Al2O3 (1%) (10) specimens, and Group (G) Polishing with Diamond Al2O3 (1.5%) (10) specimens. Data were statistically analyzed using statistical package for social science (SPSS), and the (ANOVA) test is used to determine whether the statistical hypothesis is true. Results: - For the hardness readings the higher mean value of hardness test found in group(D) (1%) polished by colloidal silica (82.74), then group (F)(1.5%)polished by colloidal(82.18), then group (F)(1%)polished by diamond( 81.12), then group(G)(1.5%)polished by diamond( 80.62),then group(C)(1.5%)polished with pumice(80.34),then group(B)(1%) polished with pumice(80.2),then at least group (A)control(80.18). Each of the three groups had a statistically significant difference with Highly sign. (P<0.01). Conclusions: -Specimens of acrylic reinforcement with adding 1.5% of Nano AL2O3 and polished with (colloidal silica, diamond suspension, and pumice, respectively) sequentially showed highly surface hardness then
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不同材料抛光后纳米 Al2O3 加固的热固化丙烯酸树脂表面硬度评估
本研究的目的是确定用纳米 Al2O3 增强的热固化丙烯酸树脂在经过各种材料抛光后的表面硬度。材料和方法:- 70 个长方形样品由粉红色抗冲击热固性丙烯酸树脂(Vertex,Implacryl,荷兰)制成(65 毫米长 x 10 毫米直径 x 3 毫米厚)。使用每种材料(浮石、金刚石悬浮液、胶体二氧化硅)抛光后,使用 Profilometer 表面粗糙度仪测定每个样品的表面粗糙度。样品表面以非常平整的位置粘在轮廓仪的水平基座上,测针(轮廓仪的针)在每个样品表面上沿三个不同方向移动三次,距离为 1.7 毫米。根据纳米粉末的浓度将试样分为 7 组:A 组为不添加纳米填料(Al2O3)的对照组(10 个试样);B 组为用浮石 Al2O3(1%)抛光的试样(10 个试样);C 组为用浮石 Al2O3(1.5 %)(10 个)试样,(D 组)用胶体 Al2O3(1%)抛光(10 个)试样,(E 组)用胶体 Al2O3(1.5%)抛光(10 个)试样,(F 组)用金刚石 Al2O3(1%)抛光(10 个)试样,以及(G 组)用金刚石 Al2O3(1.5%)抛光(10 个)试样。使用社会科学统计软件包(SPSS)对数据进行统计分析,并使用(方差分析)检验来确定统计假设是否成立。结果- 在硬度读数方面,用胶体二氧化硅抛光的(D)组(1%)的硬度测试平均值较高(82.74),然后是用胶体抛光的(F)组(1.5%)(82.18),接着是用金刚石抛光的(F)组(1%)(81.12),然后是(G)组(1.5%)金刚石抛光(80.62),然后是(C)组(1.5%)浮石抛光(80.34),然后是(B)组(1%)浮石抛光(80.2),然后至少是(A)组对照(80.18)。三组的差异均有统计学意义(Highly)(P<0.01)。(P<0.01).结论-添加了 1.5% 纳米 AL2O3 并依次用(胶体二氧化硅、金刚石悬浮液和浮石)抛光的丙烯酸加固试样显示出较高的表面硬度,然后是(A)对照组(80.2)和(B)对照组(80.18)。
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