INVESTIGATION OF THE MICROSTRUCTURE OF AISI 321 STAINLESS STEEL AFTER LASER SURFACE MELTING

Tsanka D. Dikova, Natalina K. Panova, I. Parushev
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Abstract

The aim of the present paper is to investigate the microstructure of laser-melted surface layers of austenitic steel for biomedical applications. The surface of prismatic specimens from AISI 321 stainless steel was treated by continuous CO2 laser. Three modes of laser processing were used, ensuring surface melting. The microstructure was observed by OM and SEM, while the chemical composition was investigated by EDX analysis. It was found that the microstructure of as-delivered steel was two-phase and relatively inhomogeneous in morphology and chemical composition. It consisted of austenite with grain sizes between 20 - 150 μm, relatively large amount of striped δ-ferrite and spherical carbides along the grain boundaries. After laser melting, the microstructure remained two-phase (δ-ferrite and austenite), but became more homogeneous in morphology and composition. Different dendrites morphology in the particular regions of the molten layer was confirmed - fine equiaxed dendrites on the top surface and columnar at the bottom of the molten pool. Delta-ferrite is located in the interdendritic areas and in larger amounts in the transition zone between the molten.
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激光表面熔化后 Aisi 321 不锈钢微观结构的研究
本文旨在研究用于生物医学应用的奥氏体钢激光熔化表层的微观结构。连续二氧化碳激光对 AISI 321 不锈钢棱柱试样的表面进行了处理。使用了三种激光处理模式,以确保表面熔化。通过光学显微镜和扫描电子显微镜观察了微观结构,并通过乙二胺四乙酸氧化物分析研究了化学成分。结果发现,交货钢材的微观结构为两相,形态和化学成分相对不均匀。它由晶粒大小在 20 - 150 μm 之间的奥氏体、相对较多的条纹状 δ-铁素体和沿晶界的球状碳化物组成。激光熔化后,微观结构仍为两相(δ-铁素体和奥氏体),但形态和成分变得更加均匀。熔融层特定区域的树枝状晶形态各异--在熔池顶面有细小的等轴树枝状晶,在熔池底部有柱状树枝状晶。德尔塔铁氧体位于树枝状晶间区域,在熔池与树枝状晶间的过渡区域数量较多。
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来源期刊
Journal of Chemical Technology and Metallurgy
Journal of Chemical Technology and Metallurgy Engineering-Industrial and Manufacturing Engineering
CiteScore
1.40
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