Iron oxide nanoparticles produced by the laser ablation technique and analyzed by x-ray photoelectron spectroscopy

IF 1.6 Q3 PHYSICS, CONDENSED MATTER Surface Science Spectra Pub Date : 2024-01-11 DOI:10.1116/6.0002839
E. David Gonzalez, M. Botero, R. Ospina
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Abstract

The study of iron nanoparticles is one of the most researched areas in recent times due to the potential applications they have and because the study of iron by XPS is one of the most debated elements. In this work, we provide investigation data of iron oxide nanoparticles produced using the laser ablation technique, which were characterized using x-ray photoelectron spectroscopy. Survey spectra, C 1s, O 1s, and Fe 2p core levels spectra were acquired. Results showed the presence of Fe+3 and Fe+2 elements that constitute hematite and magnetite with differences in their concentrations depending on the fitting method. In addition, the presence of adventitious carbon and carbon from impurities was detected.
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利用激光烧蚀技术制备并通过 X 射线光电子能谱进行分析的氧化铁纳米粒子
铁纳米粒子的研究是近来研究最多的领域之一,因为它们具有潜在的应用价值,也因为用 XPS 研究铁是最受争议的元素之一。在这项工作中,我们提供了使用激光烧蚀技术生产的氧化铁纳米粒子的调查数据,并使用 X 射线光电子能谱对其进行了表征。我们获得了勘测光谱、C 1s、O 1s 和 Fe 2p 核电平光谱。结果显示存在构成赤铁矿和磁铁矿的 Fe+3 和 Fe+2 元素,其浓度因拟合方法的不同而有所差异。此外,还检测到了不定碳和杂质碳的存在。
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来源期刊
Surface Science Spectra
Surface Science Spectra PHYSICS, CONDENSED MATTER-
CiteScore
1.90
自引率
7.70%
发文量
36
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