Comparison of Adhesion Performance of a Self-curing and a Light-curing Universal Adhesive to Various Dental Substrates and CAD/CAM Materials.

Cristina M P Vidal, Erica C Teixeira, Steven R Armstrong, Fang Qian
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Abstract

Purpose: To compare the adhesion of a self-curing (Tokuyama Universal Bond, TUB) and a light-curing (Scotchbond Universal, SBU) universal adhesive to CAD/CAM materials, enamel, and dentin. This study also assessed differences in enamel adhesion between self-etch vs selective etching modes, as well as immediate and long-term adhesion to dentin for both adhesives.

Materials and methods: Shear bond strength (SBS) testing was used to assess adhesion to enamel, dentin, Lava Ultimate (LU), Vita Enamic (VE), IPS e.max CAD (LD), IPS e.max ZirCAD (3Y-Zir), and Lava Esthetic (5Y-Zir) (n = 10). Moreover, bonding to enamel in self-etch and selective etching modes (n = 10) as well as immediate and aged resin-dentin bond strength (24 h after bonding, after 100,000 thermal cycles [TC] and long-term storage) was evaluated using the microtensile bond-strength test (n = 30). Failure mode was also determined for the bonding to dentin. Statistical analyses consisted of one-way and two-way ANOVA with appropriate post-hoc Tukey-Kramer or two-sample t-tests, as well as the chi-squared or Fisher's exact test (α = 0.05).

Results: TUB and SBU universal adhesives presented similar bonding to LU, VE, 3Y-Zir, and 5Y-Zir. However, SBS for TUB was superior to SBU when bonding to lithium-disilicate glass-ceramic (IPS e.max CAD). SBU showed better adhesion to dentin and enamel when used in the self-etch mode, while TUB promoted strong bond strength to enamel in the selective etching mode. TUB after TC was the only aging condition that yielded a significant reduction in resin-dentin bond strength.

Conclusion: In-vitro adhesion performance of the self-curing and light-curing universal adhesives varies depending on the dental substrate or CAD/CAM restorative material used for bonding.

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自固化和光固化通用粘合剂与各种牙科基底材料和 CAD/CAM 材料的粘合性能比较
目的:比较自固化万能粘接剂(Tokuyama Universal Bond,TUB)和光固化万能粘接剂(Scotchbond Universal,SBU)对 CAD/CAM 材料、牙釉质和牙本质的粘附性。本研究还评估了自刻蚀与选择性刻蚀模式在牙釉质粘附性方面的差异,以及两种粘合剂在牙本质上的即时和长期粘附性:剪切粘接强度(SBS)测试用于评估与牙釉质、牙本质、Lava Ultimate (LU)、Vita Enamic (VE)、IPS e.max CAD (LD)、IPS e.max ZirCAD (3Y-Zir) 和 Lava Esthetic (5Y-Zir) (n = 10)的粘接性。此外,还使用微拉伸粘接强度测试评估了自酸蚀和选择性蚀刻模式下与牙釉质的粘接(n = 10)以及即时和老化树脂-牙本质粘接强度(粘接后 24 小时、100,000 热循环 [TC] 和长期储存后)(n = 30)。还确定了与牙本质粘接的失效模式。统计分析包括单因子方差分析和双因子方差分析,并进行适当的事后Tukey-Kramer或双样本t检验,以及卡方检验或费雪精确检验(α = 0.05):TUB 和 SBU 通用粘合剂与 LU、VE、3Y-Zir 和 5Y-Zir 的粘合效果相似。不过,在与二硅酸锂玻璃陶瓷(IPS e.max CAD)粘接时,TUB 的 SBS 优于 SBU。在自酸蚀模式下,SBU 与牙本质和珐琅质的粘结力更好,而在选择性酸蚀模式下,TUB 与珐琅质的粘结力更强。在 TC 之后使用 TUB 是唯一会显著降低树脂与牙本质粘接强度的老化条件:结论:自固化和光固化通用粘合剂的体外粘合性能因牙科基底或用于粘合的 CAD/CAM 修复材料而异。
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