High-Temperature Annealing of Cermet Materials Based on Ti–C–NiCr

IF 0.3 4区 材料科学 Q4 MATERIALS SCIENCE, CERAMICS Refractories and Industrial Ceramics Pub Date : 2024-02-26 DOI:10.1007/s11148-024-00844-2
M. S. Antipov, P. M. Bazhin, A. P. Chizhikov, A. S. Konstantinov
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Abstract

Cermet materials based on titanium carbide and nichrome that were prepared by SHS extrusion were annealed in an oxidizing atmosphere at high temperatures of 800, 900, 950, and 1000°C for 10 h. Dependences of weight gain and oxidation rate of the oxidized samples on temperature and annealing time were plotted. It was found using x-ray phase analysis and scanning electron microscopy that the carbide phases did not change stoichiometry, a new CrNi3 phase was detected, and oxide films (TiO2 and Cr2O) formed on the sample surfaces. TiC carbide grains grew from 2.79 to 3.4 μm as the annealing temperature increased.

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基于 Ti-C-NiCr 的金属陶瓷材料的高温退火
用 SHS 挤压法制备的基于碳化钛和镍铬的金属陶瓷材料在 800、900、950 和 1000°C 的高温氧化气氛中退火 10 小时。利用 X 射线相分析和扫描电子显微镜发现,碳化物相的化学计量没有改变,检测到了新的 CrNi3 相,并且在样品表面形成了氧化膜(TiO2 和 Cr2O)。随着退火温度的升高,TiC 碳化物晶粒从 2.79 微米增长到 3.4 微米。
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来源期刊
Refractories and Industrial Ceramics
Refractories and Industrial Ceramics 工程技术-材料科学:硅酸盐
CiteScore
0.90
自引率
20.00%
发文量
38
审稿时长
6-12 weeks
期刊介绍: Refractories and Industrial Ceramics publishes peer-reviewed articles on the latest developments and discoveries in the field of refractory materials and ceramics, focusing on the practical aspects of their production and use. Topics covered include: Scientific Research; Raw Materials; Production; Equipment; Heat Engineering; Applications.
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