Layer-by-Layer Deposition of Chitosan/Hyaluronic Acid Polyelectrolyte Complex Coatings onto Polyester Films

IF 1 4区 化学 Q4 POLYMER SCIENCE Polymer Science, Series A Pub Date : 2024-03-25 DOI:10.1134/s0965545x2460008x
A. V. Birdibekova, E. A. Starostina, A. S. Kuryanova, N. A. Aksenova, P. S. Timashev, T. A. Akopova, T. S. Demina
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Abstract

The surface modification of polycaprolactone and polycaprolactone/polylactide mixed films was carried out by preliminary surface activation in NaOH. Subsequent layer-by-layer deposition of coatings based on polyelectrolyte complexes of the oppositely charged polysaccharides: chitosan and hyaluronic acid, was carried out. The effect of surface activation was studied using contact angle measurements, surface analysis and gravimetric data. The characterization of the polyelectrolyte complex coatings using gravimetric analysis, goniometric and micrometer measurements, scanning electron, optical and fluorescence microscopy, and FTIR-ATR spectroscopy confirmed the formation of a uniform coating with a thickness of about 30 μm, which is not prone to peeling from the substrate.

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在聚酯薄膜上逐层沉积壳聚糖/透明质酸聚电解质复合物涂层
摘要 通过在 NaOH 中进行初步表面活化,对聚己内酯和聚己内酯/聚乳酸混合薄膜进行了表面改性。随后进行了基于壳聚糖和透明质酸这两种带相反电荷的多糖的聚电解质复合物的逐层沉积。利用接触角测量、表面分析和重量数据研究了表面活化的影响。利用重量分析、测角仪和千分尺测量、扫描电子显微镜、光学显微镜和荧光显微镜以及傅立叶变换红外-ATR 光谱法对聚电解质复合物涂层进行了表征,证实形成了厚度约为 30 μm 的均匀涂层,不易从基底剥离。
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来源期刊
Polymer Science, Series A
Polymer Science, Series A 化学-高分子科学
CiteScore
1.70
自引率
0.00%
发文量
55
审稿时长
3 months
期刊介绍: Polymer Science, Series A is a journal published in collaboration with the Russian Academy of Sciences. Series A includes experimental and theoretical papers and reviews devoted to physicochemical studies of the structure and properties of polymers (6 issues a year). All journal series present original papers and reviews covering all fundamental aspects of macromolecular science. Contributions should be of marked novelty and interest for a broad readership. Articles may be written in English or Russian regardless of country and nationality of authors. All manuscripts are peer reviewed. Online submission via Internet to the Series A, B, and C is available at http://polymsci.ru.
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