Preparation of magnetic Fe3O4/PAM composite microspheres by inverse emulsion polymerization

IF 1 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Digest Journal of Nanomaterials and Biostructures Pub Date : 2024-03-26 DOI:10.15251/djnb.2024.191.435
Q. Y. Huang, S. Z. Wang, L. Dong, C. Chen, X. L. Zhao
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Abstract

The stable micro-aqueous groups (MAGs) were prepared by using sodium dodecyl sulfate (SDS) and sorbitan fatty acid ester (Span80) as emulsifiers. Fe3O4/PAM composite microspheres (CMPs) were obtained by inverse emulsion polymerization in MAGs. The experimental results showed that the size of the spherical Fe3O4/PAM CMPs was about 135-420nm and the saturation magnetization value of them was about 23.3emu/g. In the Fe3O4/PAM CMPs, the mass fraction of PAM was about 76.5%. The viscosity of the emulsion containing Fe3O4/PAM CMPs increased with the increase of current and decreased with the increase of shear rate
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利用反向乳液聚合法制备磁性 Fe3O4/PAM 复合微球
以十二烷基硫酸钠(SDS)和山梨醇脂肪酸酯(Span80)为乳化剂制备了稳定的微水团(MAGs)。Fe3O4/PAM 复合微球(CMPs)是在 MAGs 中进行反乳液聚合得到的。实验结果表明,球形 Fe3O4/PAM CMPs 的尺寸约为 135-420nm,饱和磁化值约为 23.3emu/g。在 Fe3O4/PAM CMP 中,PAM 的质量分数约为 76.5%。含有 Fe3O4/PAM CMPs 的乳液的粘度随电流的增加而增加,随剪切速率的增加而降低。
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来源期刊
Digest Journal of Nanomaterials and Biostructures
Digest Journal of Nanomaterials and Biostructures 工程技术-材料科学:综合
CiteScore
1.50
自引率
22.20%
发文量
116
审稿时长
4.3 months
期刊介绍: Under the aegis of the Academy of Romanian Scientists Edited by: -Virtual Institute of Physics operated by Virtual Company of Physics.
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