2,3,5,6-Tetrafluoro-[N-(3-aminopropyl)-ε-caprolactam]-4-pyridine

Molbank Pub Date : 2024-02-22 DOI:10.3390/m1777
Chadron M. Friesen, Nathan J. Weeks, Scott T. Iacono
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Abstract

The title compound was synthesized at a near-quantitative yield using the nucleophilic aromatic substitution of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) with perfluoropyridine (PFP). The purity and structure were determined by NMR (1H, 13C, 19F), GC-EIMS, and single-crystal X-ray crystallography.
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2,3,5,6-四氟-[N-(3-氨基丙基)-ε-己内酰胺]-4-吡啶
利用全氟吡啶(PFP)对 1,8-二氮杂双环[5.4.0]十一-7-烯(DBU)的亲核芳香取代作用,合成了标题化合物,产量接近定量。该化合物的纯度和结构是通过核磁共振(1H、13C、19F)、气相色谱-质谱和单晶 X 射线晶体学测定的。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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