SYNTHESIS AND PHYSICO-CHEMICAL STUDY OF Co, Ni, Cu, AND Sn NANOPARTICLES

Tihomir Petrov, L. Aljihmani
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Abstract

Cobalt, nickel, copper, and tin nanosized particles were synthesized through a borohydride reduction method with a reducing agent of NaBH4. The reductive precipitation was carried out at room temperature and atmospheric pressure. The nanoparticle powders were synthesized from water solutions of sulfate salts. The obtained nanosized particles were investigated by scanning electron microscopy (SEM) and XRD analyses. The SEM micrographs showed the nanoparticles’ morphology and structure. The chemical elements’ distribution was determined by energy dispersive spectroscopy (EDS) analysis. The X-ray diffraction (XRD) analysis determined the phase composition and state (amorphous or crystalline).
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钴、镍、铜和锡纳米颗粒的合成与物理化学研究
以 NaBH4 为还原剂,通过硼氢化还原法合成了钴、镍、铜和锡纳米粒子。还原沉淀在室温和常压下进行。纳米颗粒粉末由硫酸盐水溶液合成。获得的纳米颗粒通过扫描电子显微镜(SEM)和 XRD 分析进行了研究。扫描电子显微镜显微照片显示了纳米颗粒的形态和结构。通过能量色散光谱(EDS)分析确定了化学元素的分布。X 射线衍射(XRD)分析确定了相组成和状态(无定形或结晶)。
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来源期刊
Journal of Chemical Technology and Metallurgy
Journal of Chemical Technology and Metallurgy Engineering-Industrial and Manufacturing Engineering
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1.40
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