Fractionation of edible fats—Separation of fat-covered particles by decanter centrifuge

IF 1.8 3区 农林科学 Q3 FOOD SCIENCE & TECHNOLOGY European Journal of Lipid Science and Technology Pub Date : 2024-04-03 DOI:10.1002/ejlt.202300111
Myrofora Kyrimlidou, Tim Alexander Terstegen, Alessandra Parisi, Leonie Wagner, Susanne Eva Johanne Rudolph-Flöter, Eckhard Flöter
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Abstract

This work investigates the feasibility of using a decanter centrifuge to separate solid particles coated with a high melting fat from a liquid oil. The process involves feeding cold silica particles into a melt, upon which the hardstock fat crystallizes, and the particles are subsequently separated using a decanter centrifuge. Being the first attempt for such a design, only the separation step is studied, and a model system is used. It comprised canola oil (CO), fully hydrogenated rapeseed oil a priori crystallized on silica gel particles. Different particle sizes and accelerations of gravity were studied. To measure the success of this separation process, the data from light microscopy, and differential scanning calorimetry of the feed, oleins, and stearins were used. The findings show that the separation of the fatty particles used in this work, and liquid oil in decanter centrifuges is feasible while future research should focus on the crystallization part of the process. The model developed to describe the oil-holding capacity of the cake focuses on the capillary liquid entrapped in the spaces between the particles and sufficiently represents the experimental findings which show that separation efficiencies increase with increasing centrifugal acceleration.

Practical Applications: This work introduces an alternative fat fractionation process by separating a model system of CO, FHRO, and solid entrainers through a decanter centrifuge. The results can be potentially used for the development of a fully continuous dry fractionation process, which can achieve in one step higher SE than the conventional ones and can be tripalmitate-selective.

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食用脂肪的分馏--用卧螺离心机分离脂肪包裹的颗粒
这项研究探讨了使用卧螺离心机从液态油中分离涂有高熔点脂肪的固体颗粒的可行性。该工艺包括向熔体中加入冷硅石颗粒,在熔体中,硬质脂肪结晶,然后使用卧螺离心机分离颗粒。作为此类设计的首次尝试,只对分离步骤进行了研究,并使用了一个模型系统。它包括菜籽油(CO)、事先在硅胶颗粒上结晶的全氢化菜籽油。研究了不同的颗粒大小和重力加速度。为了衡量这一分离过程是否成功,使用了饲料、油脂和硬脂的光学显微镜和差示扫描量热法数据。研究结果表明,本研究中使用的脂肪颗粒与卧螺离心机中的液态油分离是可行的,而未来的研究应侧重于该过程的结晶部分。为描述滤饼的持油能力而开发的模型侧重于颗粒间隙中夹带的毛细管液体,充分体现了实验结果,即分离效率随着离心加速度的增加而提高:这项研究通过卧螺离心机分离一氧化碳、氟己烷和固体夹带物的模型系统,介绍了一种替代性脂肪分馏工艺。研究结果可用于开发一种完全连续的干法分馏工艺,该工艺可在一个步骤中实现比传统工艺更高的 SE 值,并具有三棕榈酸盐选择性。
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来源期刊
CiteScore
5.50
自引率
0.00%
发文量
101
审稿时长
6-16 weeks
期刊介绍: The European Journal of Lipid Science and Technology is a peer-reviewed journal publishing original research articles, reviews, and other contributions on lipid related topics in food science and technology, biomedical science including clinical and pre-clinical research, nutrition, animal science, plant and microbial lipids, (bio)chemistry, oleochemistry, biotechnology, processing, physical chemistry, and analytics including lipidomics. A major focus of the journal is the synthesis of health related topics with applied aspects. Following is a selection of subject areas which are of special interest to EJLST: Animal and plant products for healthier foods including strategic feeding and transgenic crops Authentication and analysis of foods for ensuring food quality and safety Bioavailability of PUFA and other nutrients Dietary lipids and minor compounds, their specific roles in food products and in nutrition Food technology and processing for safer and healthier products Functional foods and nutraceuticals Lipidomics Lipid structuring and formulations Oleochemistry, lipid-derived polymers and biomaterials Processes using lipid-modifying enzymes The scope is not restricted to these areas. Submissions on topics at the interface of basic research and applications are strongly encouraged. The journal is the official organ the European Federation for the Science and Technology of Lipids (Euro Fed Lipid).
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Cover Picture: Eur. J. Lipid Sci. Technol. 11/2024 Editorial Board: Eur. J. Lipid Sci. Technol. 11/2024 Contents: Eur. J. Lipid Sci. Technol. 11/2024 One step beyond for CNSL-based plasticizers for PVC: Use of cardol Cover Picture: Eur. J. Lipid Sci. Technol. 10/2024
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