1-(3-Chlorophenyl)-3-(6-((1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylidene)amino)hexyl)thiourea

Molbank Pub Date : 2024-04-18 DOI:10.3390/m1809
Daria Zapravdina, V. Burmistrov
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Abstract

The compound 1-(3-chlorophenyl)-3-(6-((1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylidene)amino)hexyl)thiourea was synthesized for the first time from 6-((1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylidene)amino)hexan-1-amine and 3-chlorophenylisothiocyanate in DMF with a 60% yield. It was characterized by 1H, 13C{1H} NMR, FT-IR, MS, and elemental analysis.
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1-(3-氯苯基)-3-(6-((1,7,7-三甲基双环[2.2.1]庚烷-2-亚基)氨基)己基)硫脲
首次以 6-((1,7,7-三甲基双环[2.2.1]庚烷-2-亚基)氨基)己-1-胺和 3-氯苯基异硫氰酸酯为原料,在 DMF 中合成了化合物 1-(3-氯苯基)-3-(6-((1,7,7-三甲基双环[2.2.1]庚烷-2-亚基)氨基)己基)硫脲,收率为 60%。其特征为 1H、13C{1H} NMR、FT-IR核磁共振、傅立叶变换红外光谱、质谱和元素分析对其进行了表征。
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